Evidence map›Paper›PMID 35494431›Full record

ArticleRSC advances2020

Ti-superoxide catalyzed oxidative amidation of aldehydes with saccharin as nitrogen source: synthesis of primary amides.

Rohit B Kamble, Kishor D Mane, Bapurao D Rupanawar, Pranjal Korekar, A Sudalai, Gurunath Suryavanshi

Open access · goldAbstract read
In one paragraph

Article in RSC advances, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
1.1field-weighted citation impact, top 24% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 17 citations in OpenAlex.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 2 institutions in 1 country.

Rohit B KambleChemical Engineering and Process Development Division, CSIR-National Chemical Laboratory Pune Maharashtra India-411 008 gm.suryavanshi@ncl.res.in.ORCID https://orcid.org/0000-0002-4989-6675
Kishor D ManeChemical Engineering and Process Development Division, CSIR-National Chemical Laboratory Pune Maharashtra India-411 008 gm.suryavanshi@ncl.res.in.ORCID https://orcid.org/0000-0002-4866-4557
Bapurao D RupanawarChemical Engineering and Process Development Division, CSIR-National Chemical Laboratory Pune Maharashtra India-411 008 gm.suryavanshi@ncl.res.in.ORCID https://orcid.org/0000-0002-5549-2626
Pranjal KorekarDepartment of Chemistry, MES Abasaheb Garware College Pune India-411004.
A SudalaiChemical Engineering and Process Development Division, CSIR-National Chemical Laboratory Pune Maharashtra India-411 008 gm.suryavanshi@ncl.res.in.
Gurunath SuryavanshiChemical Engineering and Process Development Division, CSIR-National Chemical Laboratory Pune Maharashtra India-411 008 gm.suryavanshi@ncl.res.in.ORCID https://orcid.org/0000-0002-6299-0914
National Chemical Laboratory · INAbasaheb Garware College · IN

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A new heterogeneous catalytic system (Ti-superoxide/saccharin/TBHP) has been developed that efficiently catalyzes oxidative amidation of aldehydes to produce various primary amides. The protocol employs saccharin as amine source and was found to tolerate a wide range of substrates with different functional groups. Moderate to excellent yields, catalyst reusability and operational simplicity are the main highlights. A possible mechanism and the role of the catalyst in oxidative amidation have also been discussed.

Identifiers

PMID35494431
PMCPMC9047451
OpenAlexW2997555293

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.