Evidence map›Paper›PMID 35366707›Full record

ArticleMikrochimica acta2022

3D printed spinning cup-shaped device for immunoaffinity solid-phase extraction of diclofenac in wastewaters.

Enrique Javier Carrasco-Correa, José Manuel Herrero-Martínez, Ernesto Francisco Simó-Alfonso, Dietmar Knopp, Manuel Miró

Open access · hybridAbstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Mikrochimica acta, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
1.6field-weighted citation impact, top 18% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 25 citations in OpenAlex.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 3 institutions in 2 countries.

Enrique Javier Carrasco-CorreaCLECEM group, Department of Analytical Chemistry, University of Valencia, University of Valencia, C/Doctor Moliner 50, 46100, Burjassot Valencia, Spain. enrique.carrasco@uv.es.
José Manuel Herrero-MartínezCLECEM group, Department of Analytical Chemistry, University of Valencia, University of Valencia, C/Doctor Moliner 50, 46100, Burjassot Valencia, Spain.
Ernesto Francisco Simó-AlfonsoCLECEM group, Department of Analytical Chemistry, University of Valencia, University of Valencia, C/Doctor Moliner 50, 46100, Burjassot Valencia, Spain.
Dietmar KnoppDepartment of Chemistry, Technical University of Munich, Elisabeth-Winterhalter Str. 6, 83177, München, Germany.
Manuel MiróFI-TRACE Group, Department of Chemistry, University of Balearic Islands, Carretera de Valldemossa, km 7.5, 07122, Palma de Mallorca, Spain. manuel.miro@uib.es.ORCID http://orcid.org/0000-0002-8413-3008
Universitat de València · ESTechnical University of Munich · DEUniversitat de les Illes Balears · ES

Funding

Ministerio de Ciencia, Innovación y Universidades PID2020-117686RB-C33Ministerio de Ciencia, Innovación y Universidades RTI2018-095536-B-I00Secretaría de Estado de Investigación, Desarrollo e Innovación RED2018-102522-T
6 · The paper itself

Abstract

This article reports current research efforts towards designing bespoke microscale extraction approaches exploiting the versatility of 3D printing for fast prototyping of novel geometries of sorptive devices. This is demonstrated via the so-called 3D printed spinning cup-based platform for immunoextraction of emerging contaminants using diclofenac as a model analyte. A new format of rotating cylindrical scaffold (containing a semispherical upper cavity) with enhanced coverage of biorecognition elements, and providing elevated enhancement factors with no need of eluate processing as compared with other microextraction stirring units is proposed. Two distinct synthetic routes capitalized upon modification of the acrylate surface of stereolithographic 3D printed parts with hexamethylenediamine or branched polyethyleneimine chemistries were assayed for covalent binding of monoclonal diclofenac antibody.Under the optimized experimental conditions, a LOD of 108 ng L

Indexed as

DiclofenacWastewaterChromatography, LiquidPrinting, Three-DimensionalSolid Phase ExtractionDiclofenacWastewater3D printingDiclofenacExtraction deviceImmunosorbentWastewater

Identifiers

PMID35366707
PMCPMC8976768
OpenAlexW4225151219

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.