ArticleScientific reports2022
Tandem oxidative amidation of benzylic alcohols by copper(II) supported on metformin-graphitic carbon nitride nanosheets as an efficient catalyst.
Article in Scientific reports, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.
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8 citing papers in PubMed, 24 citations in OpenAlex.
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- Ionic liquid-functionalized magnetic polystyrene nanoparticles for efficient removal of methyl violet and acid red 88 from aqueous media.Scientific reports · 2025Article
- Tetrazole derivatives synthesisRSC advances · 2025Article
- Bifunctionalised acid-base hierarchically structured monolithic microreactor for continuous-flow tandem catalytic process of cyanocinnamate synthesis.Scientific reports · 2024Article
- Synthesis and characterization of nanocatalyst CuScientific reports · 2023Article
- Article
- Coupling photocatalytic water oxidation with reductive transformations of organic molecules.Nature communications · 2022Article
- Heteroployacid on the composite of boehmite and polyionic liquid as a catalyst for alcohol oxidation and tandem alcohol oxidation Knoevenagel condensation reactions.Scientific reports · 2022Article
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3 authors at 1 institution in 1 country.
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Abstract
In this research, an efficient heterogeneous catalyst based on graphitic carbon nitride nanosheets (CN) has been reported. The CN was functionalized by 1,3-dibromopropane as a linker (CN-Pr-Br) and subsequently modified with metformin (CN-Pr-Met). Furthermore, the copper(II) was coordinated on modified CN (CN-Pr-Met-Cu(II)) and during this process, 7.94% copper(II) was loaded into the catalyst structure. The synthesized catalyst was evaluated by various techniques including fourier-transform infrared spectroscopy (FT-IR), energy dispersive X-ray spectroscopy (EDS), field emission scanning electron microscopy (FE-SEM), thermogravimetric analysis (TGA), X-ray diffraction (XRD), and inductively coupled plasma atomic emission spectroscopy (ICP-OES). CN-Pr-Met-Cu(II) was used as a catalyst in the synthesis of amides via the oxidation of benzyl alcohols. The conditions of this reaction were optimized in terms of temperature, time, amount of catalyst, type of base, oxidant, and solvent. Moreover, a variety of amides with an efficiency of 75-95% were synthesized. The reaction was carried out in the presence of benzyl alcohols, amine hydrochloride salts, tert-butyl hydroperoxide (TBHP), CaCO
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