Evidence map›Paper›PMID 35254295›Full record

ArticleJournal of synchrotron radiation2022

3D printed devices and infrastructure for liquid sample delivery at the European XFEL.

Mohammad Vakili, Johan Bielecki, Juraj Knoška, Florian Otte, Huijong Han, Marco Kloos, Robin Schubert, Elisa Delmas, Grant Mills, Raphael de Wijn and 11 more

Abstract read
In one paragraph

Article in Journal of synchrotron radiation, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 35 papers.

0numbers the graph read from it
0cells of the map it votes in
35citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

35 citing papers in PubMed.

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  18. A snapshot love story: what serial crystallography has done and will do for us.Acta crystallographica. Section D, Structural biology · 2024
    Review
  19. Article
  20. SARS-CoV-2 MNature communications · 2024
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

21 authors.

Mohammad VakiliEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-9776-0177
Johan BieleckiEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-3012-603X
Juraj KnoškaCenter for Free-Electron Laser Science (CFEL), Deutsches Elektronen-Synchrotron (DESY), Notkestrasse 85, 22607 Hamburg, Germany.ORCID 0000-0001-7258-6256
Florian OtteEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-2431-4464
Huijong HanEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-1197-3014
Marco KloosEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-8745-9740
Robin SchubertEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-6213-2872
Elisa DelmasEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0003-0882-0006
Grant MillsEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-9653-452X
Raphael de WijnEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-8342-1008
Romain LetrunEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-0569-5193
Simon DoldEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-5332-8251
Richard BeanEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-8151-7439
Adam RoundEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-0723-8228
Yoonhee KimEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-9209-9500
Frederico A LimaEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-8106-2892
Katerina DörnerEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0003-1072-5905
Joana ValerioEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0001-5931-0925
Michael HeymannInstitute for Biomaterials and Biomolecular Systems (IBBS), University of Stuttgart, Pfaffenwaldring 57, 70569 Stuttgart, Germany.ORCID 0000-0002-9278-8207
Adrian P MancusoEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0003-1710-8969
Joachim SchulzEuropean XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.ORCID 0000-0002-9310-8832

Funding

Deutsche Forschungsgemeinschaft The Hamburg Centre of Ultrafast Imaging (CUI)Federal Ministry of Education and Research of Germany BMBF 05K16PE1
6 · The paper itself

Abstract

The Sample Environment and Characterization (SEC) group of the European X-ray Free-Electron Laser (EuXFEL) develops sample delivery systems for the various scientific instruments, including systems for the injection of liquid samples that enable serial femtosecond X-ray crystallography (SFX) and single-particle imaging (SPI) experiments, among others. For rapid prototyping of various device types and materials, sub-micrometre precision 3D printers are used to address the specific experimental conditions of SFX and SPI by providing a large number of devices with reliable performance. This work presents the current pool of 3D printed liquid sample delivery devices, based on the two-photon polymerization (2PP) technique. These devices encompass gas dynamic virtual nozzles (GDVNs), mixing-GDVNs, high-viscosity extruders (HVEs) and electrospray conical capillary tips (CCTs) with highly reproducible geometric features that are suitable for time-resolved SFX and SPI experiments at XFEL facilities. Liquid sample injection setups and infrastructure on the Single Particles, Clusters, and Biomolecules and Serial Femtosecond Crystallography (SPB/SFX) instrument are described, this being the instrument which is designated for biological structure determination at the EuXFEL.

Indexed as

LasersPrinting, Three-DimensionalCrystallography, X-RayViscosityX-RaysaerosolscrystallographyFEL physicshigh-viscosity extrusioninstrumentationliquid jetsmicrofluidicsrapid mixingsample deliverysingle-particle imagingX-ray scattering

Identifiers

PMID35254295
PMCPMC8900844

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.