ArticleFrontiers in molecular biosciences2021
Crystalline Sponge Method by Three-Dimensional Electron Diffraction.
Article in Frontiers in molecular biosciences, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.
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Who cites it
5 citing papers in PubMed.
- Acyclic cucurbituril as sequestrant for acetaminophen.Chemical communications (Cambridge, England) · 2026Article
- Automated Nanocrystalline Sponge Workflow Enabled by 3D Electron Diffraction.Journal of the American Chemical Society · 2026Article
- A flexible copper MOF as a carboxylate-specific crystalline sponge for structure solution using X-ray and electron diffraction.Chemical science · 2026Article
- Highly Luminescent Crystalline Sponge: Sensing Properties and Direct X-ray Visualization of the Substrates.Molecules (Basel, Switzerland) · 2022Article
- Direct Location of Organic Molecules in Framework Materials by Three-Dimensional Electron Diffraction.Journal of the American Chemical Society · 2022Article
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Authors and funding
6 authors.
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Abstract
The crystalline sponge method has shown to be a novel strategy for the structure determination of noncrystalline, oily, or trace amount of a compound. A target compound was absorbed and oriented orderly in the pregrown porous crystal for x-ray diffraction analysis. However, the diffusion in the micron-sized crystals is rather difficult. Lots of trial-and-error experiments are needed to optimize the guest-soaking process and to improve data quality. Nanocrystals are better in diffusion, yet it could not conduct a single crystal x-ray diffraction (SCXRD) analysis. Three-dimensional electron diffraction (3D-ED) is a powerful diffraction tool for the structure determination of small crystals. In this work, we successfully carried out the crystalline sponge method by 3D-ED technique using {(ZnI
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