ArticleACS applied polymer materials2022
Electrochemically Initiated Synthesis of Polyacrylamide Microgels and Core-shell Particles.
Article in ACS applied polymer materials, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.
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Who cites it
1 citing paper in PubMed.
- Development of an injectable thermosensitive hydrogel depot system for controlled and sustained subcutaneous drug delivery.International journal of pharmaceutics: X · 2026Article
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Authors and funding
5 authors.
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Abstract
Herein, we developed a simple procedure for synthesizing micrometer-sized microgel particles as a suspension in an aqueous solution and thin films deposited as shells on different inorganic cores. A sufficiently high constant potential was applied to the working electrode to commence the initiator decomposition that resulted in gelation. Under hydrodynamic conditions, this initiation allowed preparing different morphology microgels at room temperature. Importantly, neither heating nor UV-light illumination was needed to initiate the polymerization. Moreover, thin films of the cross-linked gel were anchored on different core substrates, including silica and magnetic nanoparticles. Scanning electron microscopy and transmission electron microscopy imaging confirmed the microgel particles' and films' irregular shape and porous structure. Energy-dispersive X-ray spectroscopy indicated that the core coating with the microgel film was successful. Dynamic light scattering measured the micrometer size of gel particles with different combinations of acrylic monomers. Thermogravimetric analysis and the first-derivative thermogravimetric analysis revealed that the microgels' thermal stability of different compositions was different. Fourier-transform infrared and
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Registered trials
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