Evidence map›Paper›PMID 35000010›Full record

ArticleMikrochimica acta2022

Stir bar sorptive-dispersive microextraction by a poly(methacrylic acid-co-ethylene glycol dimethacrylate)-based magnetic sorbent for the determination of tricyclic antidepressants and their main active metabolites in human urine.

Víctor Vállez-Gomis, Sara Exojo-Trujillo, Juan L Benedé, Alberto Chisvert, Amparo Salvador

Open access · hybridAbstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Mikrochimica acta, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
2.0field-weighted citation impact, top 14% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 21 citations in OpenAlex.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 1 institution in 1 country.

Víctor Vállez-GomisGICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.
Sara Exojo-TrujilloGICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.
Juan L BenedéGICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.
Alberto ChisvertGICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain. alberto.chisvert@uv.es.ORCID http://orcid.org/0000-0003-1349-0478
Amparo SalvadorGICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.
Universitat de València · ES

Funding

Spanish Ministry of Science and Innovation PID2020-118924RB-I00
6 · The paper itself

Abstract

A poly(methacrylic acid-co-ethylene glycol dimethacrylate)-based magnetic sorbent was used for the rapid and sensitive determination of tricyclic antidepressants and their main active metabolites in human urine. This material was characterized by magnetism measurements, zeta potential, scanning electron microscopy, nitrogen adsorption-desorption isotherms, and thermogravimetric analysis. The proposed analytical method is based on stir bar sorptive-dispersive microextraction (SBSDME) followed by liquid chromatography-tandem mass spectrometry. The main parameters involved in the extraction step were optimized by using the response surface methodology as a multivariate optimization method, whereas a univariate approach was employed to study the desorption parameters. Under the optimized conditions, the proposed method was properly validated showing good linearity (at least up to 50 ng mL

Indexed as

Antidepressive Agents, TricyclicPolymethacrylic AcidsSolid Phase MicroextractionChromatography, LiquidCobaltEthylene GlycolsFerric CompoundsHumansMagnetic PhenomenaMethacrylatesSilicon DioxideTandem Mass SpectrometryAntidepressive Agents, TricyclicCobaltcobalt ferriteEthylene GlycolsFerric CompoundsMethacrylatespoly((ethylene glycol dimethacrylate)-co-(methacrylic acid))poly(methacrylic acid-ethylene glycol dimethacrylate)Polymethacrylic AcidsSilicon DioxideActive metabolitesHuman urineMagnetic nanoparticlesPolymeric sorbentStir bar sorptive-dispersive microextractionTricyclic antidepressants

Identifiers

PMID35000010
PMCPMC8742809
OpenAlexW4206389978

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.