ArticleJournal of synchrotron radiation2022
Implementation of cryogenic tender X-ray HR-XANES spectroscopy at the ACT station of the CAT-ACT beamline at the KIT Light Source.
Article in Journal of synchrotron radiation, 2022. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.
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Who cites it
5 citing papers in PubMed, 11 citations in OpenAlex.
- Structural and physical investigation of ordered BaO-deficient BaCommunications chemistry · 2025Article
- Resonant inelastic X-ray scattering tools to count 5 f electrons of actinides and probe bond covalency.Nature communications · 2025Article
- Np(V) Retention at the Illite du Puy Surface.Environmental science & technology · 2023Article
- Synthesis, Characterization, and Stability of Two Americium Vanadates, AmVOInorganic chemistry · 2023Article
- Foreword to the special virtual issue on Actinide physics and chemistry with synchrotron radiation.Journal of synchrotron radiation · 2022Article
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Authors and funding
8 authors at 1 institution in 1 country.
Funding
Abstract
The ACT experimental station of the CAT-ACT wiggler beamline at the Karlsruhe Institute of Technology (KIT) Light Source is dedicated to the investigation of radionuclide materials with radioactivities up to 1000000 times the exemption limit by various speciation techniques applying monochromatic X-rays. In this article, the latest technological developments at the ACT station that enable high-resolution X-ray absorption near-edge structure (HR-XANES) spectroscopy for low radionuclide loading samples are highlighted - encompassing the investigation of actinide elements down to 1 p.p.m. concentration - combined with a cryogenic sample environment reducing beam-induced sample alterations. One important part of this development is a versatile gas tight plexiglass encasement ensuring that all beam paths in the five-analyzer-crystal Johann-type X-ray emission spectrometer run within He atmosphere. The setup enables the easy exchange between different experiments (conventional X-ray absorption fine structure, HR-XANES, high-energy or wide-angle X-ray scattering, tender to hard X-ray spectroscopy) and opens up the possibility for the investigation of environmental samples, such as specimens containing transuranium elements from contaminated land sites or samples from sorption and diffusion experiments to mimic the far field of a breached nuclear waste repository.
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