ArticlePolymers2021
Rosin-Based Epoxy Vitrimers with Dynamic Boronic Ester Bonds.
Article in Polymers, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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Who cites it
14 citing papers in PubMed, 80 citations in OpenAlex.
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- A review on the formulation and performance of epoxidized vegetable oil-based vitrimer: stoichiometric calculations, curing agent functionalities and catalyst efficiency.Royal Society open science · 2025Review
- Unlocking Dual Recycling in Photo-Curable Polycyanurate Thermosets Derived from Bio-Resources.Angewandte Chemie (International ed. in English) · 2025Article
- Chemical and Solvent-Based Recycling of DGEBA-Based Epoxy Thermoset and Carbon-Fiber Reinforced Epoxy Composite Utilizing Imine-Containing Secondary Amine Hardener.Macromolecular rapid communications · 2025Article
- Recent Development of Functional Bio-Based Epoxy Resins.Molecules (Basel, Switzerland) · 2024Review
- Article
- Use of Bio-Epoxies and Their Effect on the Performance of Polymer Composites: A Critical Review.Polymers · 2023Review
- A Comparative Study on the Properties of Rosin-Based Epoxy Resins with Different Flexible Chains.Polymers · 2023Article
- A Self-Healing Thermoset Epoxy Modulated by Dynamic Boronic Ester for Powder Coating.Polymers · 2023Article
- Preparation of Epoxy Resin with Disulfide-Containing Curing Agent and Its Application in Self-Healing Coating.Materials (Basel, Switzerland) · 2023Article
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- Hydroxyl-Terminated Polybutadiene-Based Polyurethane with Self-Healing and Reprocessing Capabilities.ACS omega · 2022Article
Corrections and comments
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Authors and funding
4 authors at 1 institution in 1 country.
Funding
Abstract
Rosin is an abundantly available natural product. In this paper, for the first time, a rosin derivative is employed as the main monomer for preparation of epoxy vitrimers to improve the mechanical properties of vitrimers. Novel epoxy vitrimer networks with dynamic reversible covalent boronic ester bonds are constructed by a reaction between thiols in 2,2'-(1,4-phenylene)-bis (4-mercaptan-1,3,2-dioxaborolane) (BDB) as a curing agent and epoxy groups in the rosin derivative. The rosin-based epoxy vitrimer networks are fully characterized by Fourier transform infrared spectroscopy (FTIR), an equilibrium swelling experiment, and dynamic mechanical analysis (DMA). The obtained rosin-based epoxy vitrimers possess superior thermostability and good mechanical properties. Due to transesterification of boronic ester bonds, rosin epoxy vitrimer network topologies can be altered, giving welding, recycle, self-healing, and shape memory abilities to the fabricated polymer. Besides, the effects of treating time and temperature on welding capability is investigated, and it is found that the welding efficiency of the 20% C-FPAE sample is >93% after treatment for 12 h at 160 °C. Moreover, through a hot press, the pulverized samples of 20% C-FPAE can be reshaped several times and most mechanical properties are restored after reprocessing at 200 °C for 60 min. Finally, chemical degradation is researched for the rosin-based epoxy vitrimers.
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Registered trials
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