ArticleFoods (Basel, Switzerland)2021
Comparison of Automated Extraction Techniques for Volatile Analysis of Whole Milk Powder.
Article in Foods (Basel, Switzerland), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers, 1 of them a synthesis that pooled it.
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Who cites it
11 citing papers in PubMed, 1 synthesis or guideline pooled it.
- Urinary and cellular volatile organic compounds as biomarkers for urological cancers: a systematic review of GC-MS-based volatolomics.Metabolomics : Official journal of the Metabolomic Society · 2026Pooled it
- Discrimination and characterization analysis of key flavor compounds from TianshuiFood chemistry: X · 2025Article
- Analysis of volatile organic compounds in Korean-bred strawberries: insights for improving fruit flavor.Frontiers in plant science · 2024Article
- Analysis for different flavor compounds in mature milk from human and livestock animals by GC × GC-TOFMS.Food chemistry: X · 2023Article
- Characterization and Discrimination of Volatile Compounds in Chilled Tan Mutton Meat during Storage Using HiSorb-TD-GC-MS and E-Nose.Molecules (Basel, Switzerland) · 2023Article
- Application of Direct Thermal Desorption-Gas Chromatography-Mass Spectrometry for Determination of Volatile and Semi-Volatile Organosulfur Compounds in Onions: A Novel Analytical Approach.Pharmaceuticals (Basel, Switzerland) · 2023Article
- Validation of volatile metabolites of pulmonary oxidative injury: a bench to bedside study.ERJ open research · 2023Article
- Multi-Analytical Approach to Characterize the Degradation of Different Types of Microplastics: Identification and Quantification of Released Organic Compounds.Molecules (Basel, Switzerland) · 2023Article
- A Complete Pipeline for Untargeted Urinary Volatolomic Profiling with Sorptive Extraction and Dual Polar and Nonpolar Column Methodologies Coupled with Gas Chromatography Time-of-Flight Mass Spectrometry.Analytical chemistry · 2023Article
- Exploring the Volatiles Released from Roots of Wild and Domesticated Tomato Plants under Insect Attack.Molecules (Basel, Switzerland) · 2022Article
- The Influence of Pasture and Non-pasture-Based Feeding Systems on the Aroma of Raw Bovine Milk.Frontiers in nutrition · 2022Article
Corrections and comments
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Authors and funding
6 authors.
Funding
Abstract
Volatile profiling of whole milk powder is valuable for obtaining information on product quality, adulteration, legislation, shelf life, and aroma. For routine analysis, automated solventless volatile extraction techniques are favored due their simplicity and versatility, however no single extraction technique can provide a complete volatile profile due to inherent chemical bias. This study was undertaken to compare and contrast the performance of headspace solid phase microextraction, thermal desorption, and HiSorb (a sorptive extraction technique in both headspace and direct immersion modes) for the volatile analysis of whole milk powder by gas chromatography mass spectrometry. Overall, 85 unique volatiles were recovered and identified, with 80 extracted and identified using a non-polar gas chromatography column, compared to 54 extracted, and identified using a polar gas chromatography column. The impact of salting out was minimal in comparison to gas chromatography column polarity and the differences between the extraction techniques. HiSorb extracted the most and greatest abundance of volatiles, but was heavily influenced by the number and volume of lactones extracted in comparison to the other techniques. HiSorb extracted significantly more volatiles by direct immersion than by headspace. The differences in volatile selectivity was evident between the techniques and highlights the importance of using multiple extraction techniques in order to obtain a more complete volatile profile. This study provides valuable information on the volatile composition of whole milk powder and on differences between extraction techniques under different conditions, which can be extrapolated to other food and beverages.
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