ArticlePolymers2021
Surface Analyses of PVDF/NMP/[EMIM][TFSI] Solid Polymer Electrolyte.
Article in Polymers, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.
What it found
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Who cites it
7 citing papers in PubMed, 34 citations in OpenAlex.
- Reliable characterization of polymer electrolytes for next-generation energy storage: misinterpretations, challenges, and methodological solutions.RSC advances · 2026Review
- Electro-Co-Polymerisation of Polypyrrole-Polyaniline Composites in Ionic Liquids for Metal-Free Hydrogen Evolution Electrodes.ChemistryOpen · 2024Article
- Sustainable Collagen Blends with Different Ionic Liquids for Resistive Touch Sensing Applications.ACS sustainable chemistry & engineering · 2023Article
- Piezo-Enhanced Photocatalytic Activity of the Electrospun Fibrous Magnetic PVDF/BiFeOPolymers · 2023Article
- Brief Review of PVDF Properties and Applications Potential.Polymers · 2022Review
- Solvent Evaporation Rate as a Tool for Tuning the Performance of a Solid Polymer Electrolyte Gas Sensor.Polymers · 2022Article
- Structure Tuning and Electrical Properties of Mixed PVDF and Nylon Nanofibers.Materials (Basel, Switzerland) · 2021Article
Corrections and comments
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Authors and funding
6 authors at 4 institutions in 1 country.
Funding
Abstract
Thermal treatment conditions of solid polymer polymer electrolyte (SPE) were studied with respect to their impact on the surface morphology, phase composition and chemical composition of an imidazolium ionic-liquid-based SPE, namely PVDF/NMP/[EMIM][TFSI] electrolyte. These investigations were done using scanning electron microscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, differential scanning calorimetry as well as X-ray photoelectron spectroscopy and time-of-flight secondary ion mass spectroscopy. A thoroughly mixed blend of polymer matrix, ionic liquid and solvent was deposited on a ceramic substrate and was kept at a certain temperature for a specific time in order to achieve varying crystallinity. The morphology of all the electrolytes consists of spherulites whose average diameter increases with solvent evaporation rate. Raman mapping shows that these spherulites have a semicrystalline structure and the area between them is an amorphous region. Analysis of FTIR spectra as well as Raman spectroscopy showed that the β-phase becomes dominant over other phases, while DSC technique indicated decrease of crystallinity as the solvent evaporation rate increases. XPS and ToF-SIMS indicated that the chemical composition of the surface of the SPE samples with the highest solvent evaporation rate approaches the composition of the ionic liquid.
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Registered trials
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