Evidence map›Paper›PMID 34123303›Full record

ArticleChemical science2020

Manometric real-time studies of the mechanochemical synthesis of zeolitic imidazolate frameworks.

Ivana Brekalo, Wenbing Yuan, Cristina Mottillo, Yuneng Lu, Yuancheng Zhang, Jose Casaban, K Travis Holman, Stuart L James, Frédéric Duarte, P Andrew Williams and 2 more

Abstract read
In one paragraph

Article in Chemical science, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 26 papers, 1 of them a synthesis that pooled it.

0numbers the graph read from it
0cells of the map it votes in
26citing papers in PubMed, 1 pooled it
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

26 citing papers in PubMed, 1 synthesis or guideline pooled it.

  1. Pooled it
  2. Article
  3. Review
  4. Review
  5. Article
  6. Article
  7. Article
  8. Article
  9. Review
  10. Article
  11. Article
  12. Time-Resolved In Situ Monitoring of Mechanochemical Reactions.Angewandte Chemie (International ed. in English) · 2022
    Review
  13. Article
  14. Mechanochemical vs Wet Approach for Directing COACS sustainable chemistry & engineering · 2022
    Article
  15. Article
  16. Article
  17. Mechanochemical Grignard Reactions with Gaseous COAngewandte Chemie (International ed. in English) · 2022
    Article
  18. Review
  19. Article
  20. Orbital Mapping of Semiconducting Perylenes on Cu(111).The journal of physical chemistry. C, Nanomaterials and interfaces · 2021
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

12 authors.

Ivana BrekaloDepartment of Chemistry, Georgetown University 20057 Washington, D.C. USA kth7@georgetown.edu.ORCID https://orcid.org/0000-0002-0309-5610
Wenbing YuanSchool of Enviromental and Chemical Engineering, Foshan University Foshan 528000 China.
Cristina MottilloDepartment of Chemistry, McGill University H3A 0B8 Montreal Quebec Canada tomislav.friscic@mcgill.ca.
Yuneng LuDepartment of Chemistry, McGill University H3A 0B8 Montreal Quebec Canada tomislav.friscic@mcgill.ca.
Yuancheng ZhangSchool of Chemistry, Queen's University Belfast BT7 1NN Belfast UK S.James@qub.ac.uk.
Jose CasabanMOF Technologies BT7 1NF Belfast UK.
K Travis HolmanDepartment of Chemistry, Georgetown University 20057 Washington, D.C. USA kth7@georgetown.edu.ORCID https://orcid.org/0000-0003-1800-300X
Stuart L JamesSchool of Chemistry, Queen's University Belfast BT7 1NN Belfast UK S.James@qub.ac.uk.ORCID https://orcid.org/0000-0002-6554-0345
Frédéric DuarteSchool of Chemistry, Cardiff University CF10 3AT Cardiff UK HarrisKDM@cardiff.ac.uk.
P Andrew WilliamsSchool of Chemistry, Cardiff University CF10 3AT Cardiff UK HarrisKDM@cardiff.ac.uk.
Kenneth D M HarrisSchool of Chemistry, Cardiff University CF10 3AT Cardiff UK HarrisKDM@cardiff.ac.uk.ORCID https://orcid.org/0000-0001-7855-8598
Tomislav FriščićDepartment of Chemistry, McGill University H3A 0B8 Montreal Quebec Canada tomislav.friscic@mcgill.ca.ORCID https://orcid.org/0000-0002-3921-7915

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

We demonstrate a simple method for real-time monitoring of mechanochemical synthesis of metal-organic frameworks, by measuring changes in pressure of gas produced in the reaction. Using this manometric method to monitor the mechanosynthesis of the zeolitic imidazolate framework ZIF-8 from basic zinc carbonate reveals an intriguing feedback mechanism in which the initially formed ZIF-8 reacts with the CO

Identifiers

PMID34123303
PMCPMC8150112

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.