ArticleAdvanced materials (Deerfield Beach, Fla.)2021
In Situ TEM Imaging of Solution-Phase Chemical Reactions Using 2D-Heterostructure Mixing Cells.
Article in Advanced materials (Deerfield Beach, Fla.), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 10 papers.
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Who cites it
10 citing papers in PubMed.
- In Situ Liquid-Cell Transmission Electron Microscopy Insights Into Lithium-Ion Battery Materials Degradation: Challenges and Emerging Solutions.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2026Review
- Graphene-Based Liquid Cell Designs for In Situ Liquid-Phase Transmission Electron Microscopy: Recent Developments and Perspectives.Small science · 2025Review
- Influence of Nanobubbles on the Early Stages of Calcium Carbonate Formation.Crystal growth & design · 2025Article
- Real-time visualisation of fast nanoscale processes during liquid reagent mixing by liquid cell transmission electron microscopy.Communications chemistry · 2025Article
- Exploring Biomineralization Processes Using In Situ Liquid Transmission Electron Microscopy: A Review.Small (Weinheim an der Bergstrasse, Germany) · 2025Review
- Formation, chemical evolution and solidification of the dense liquid phase of calcium (bi)carbonate.Nature materials · 2025Article
- Toward sub-second solution exchange dynamics in flow reactors for liquid-phase transmission electron microscopy.Nature communications · 2024Article
- Review
- Goethite Mineral Dissolution to Probe the Chemistry of Radiolytic Water in Liquid-Phase Transmission Electron Microscopy.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2023Article
- In Situ TEM Imaging of Solution-Phase Chemical Reactions Using 2D-Heterostructure Mixing Cells.Advanced materials (Deerfield Beach, Fla.) · 2021Article
Corrections and comments
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Authors and funding
6 authors.
Funding
Abstract
Liquid-phase transmission electron microscopy is used to study a wide range of chemical processes, where its unique combination of spatial and temporal resolution provides countless insights into nanoscale reaction dynamics. However, achieving sub-nanometer resolution has proved difficult due to limitations in the current liquid cell designs. Here, a novel experimental platform for in situ mixing using a specially developed 2D heterostructure-based liquid cell is presented. The technique facilitates in situ atomic resolution imaging and elemental analysis, with mixing achieved within the immediate viewing area via controllable nanofracture of an atomically thin separation membrane. This novel technique is used to investigate the time evolution of calcium carbonate synthesis, from the earliest stages of nanodroplet precursors to crystalline calcite in a single experiment. The observations provide the first direct visual confirmation of the recently developed liquid-liquid phase separation theory, while the technological advancements open an avenue for many other studies of early stage solution-phase reactions of great interest for both the exploration of fundamental science and developing applications.
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Registered trials
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