Evidence map›Paper›PMID 34066906›Full record

ArticleMicromachines2021

Fabrication of X-ray Gratings for Interferometric Imaging by Conformal Seedless Gold Electroplating.

Konstantins Jefimovs, Joan Vila-Comamala, Carolina Arboleda, Zhentian Wang, Lucia Romano, Zhitian Shi, Matias Kagias, Marco Stampanoni

Abstract read
In one paragraph

Article in Micromachines, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 10 papers.

0numbers the graph read from it
0cells of the map it votes in
10citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

10 citing papers in PubMed.

  1. Microfluidic Gratings for X-Ray Phase Contrast Imaging.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2026
    Article
  2. Article
  3. Review
  4. Article
  5. Article
  6. Article
  7. Robust Bottom-Up Gold Filling of Deep Trenches and Gratings.Journal of the Electrochemical Society · 2022
    Article
  8. Article
  9. Article
  10. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Konstantins JefimovsPaul Scherrer Institut, 5232 Villigen, Switzerland.ORCID 0000-0002-1888-0777
Joan Vila-ComamalaPaul Scherrer Institut, 5232 Villigen, Switzerland.ORCID 0000-0002-1543-3146
Carolina ArboledaPaul Scherrer Institut, 5232 Villigen, Switzerland.
Zhentian WangPaul Scherrer Institut, 5232 Villigen, Switzerland.
Lucia RomanoPaul Scherrer Institut, 5232 Villigen, Switzerland.ORCID 0000-0002-7696-7643
Zhitian ShiPaul Scherrer Institut, 5232 Villigen, Switzerland.ORCID 0000-0003-0539-219X
Matias KagiasPaul Scherrer Institut, 5232 Villigen, Switzerland.ORCID 0000-0003-0435-6672
Marco StampanoniPaul Scherrer Institut, 5232 Villigen, Switzerland.

Funding

Fondazione Gelu TACI-C ProjectH2020 European Research Council ERC-2012-StG 310005 "PhaseX"Horizon 2020 Framework Programme Eurostars Grant E!1106 "INFORMAT"Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung CRSII5_183568 "GI-BCT"Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung SNF R'Equip grant 206021_177036/1Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung SNF_R'Equip grant 206021_189662 "SiDRY"Schweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung SNF-Sinergia CRS112-154472 "MedXPhase"SwissLOS Fond of the Kanton Aargau Entwicklung einer neuartigen Röntgentechnik für die Brustkrebsdiagnose
6 · The paper itself

Abstract

We present a method to produce small pitch gratings for X-ray interferometric imaging applications, allowing the phase sensitivity to be increased and/or the length of the laboratory setup to be minimized. The method is based on fabrication of high aspect ratio silicon microstructures using deep reactive ion etching (Bosch technique) of dense grating arrays and followed by conformal electroplating of Au. We demonstrated that low resistivity Si substrates (<0.01 Ohm·cm) enable the metal seeding layer deposition step to be avoided, which is normally required to initiate the electroplating process. Etching conditions were optimized to realize Si recess structures with a slight bottom tapering, which ensured the void-free Au filling of the trenches. Vapor HF was used to remove the native oxide layer from the Si grating surface prior to electroplating in the cyanide-based Au electrolyte. Fabrication of Au gratings with pitch in the range 1.2-3.0 µm was successfully realized. A substantial improved aspect ratio of 45:1 for a pitch size of 1.2 µm was achieved with respect to the prior art on 4-inch wafer-based technology. The fabricated Au gratings were tested with X-ray interferometers in Talbot-Laue configuration with measured visibility of 13% at an X-ray design energy of 26 keV.

Indexed as

Bosch processdeep reactive ion etchinggoldgratinghigh aspect ratiophase contrast imagingseedless electroplatingsiliconvisibilityX-ray interferometry

Identifiers

PMID34066906
PMCPMC8147938

What OpenQuestion holds

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LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.