ArticleThe Journal of organic chemistry2021
Mechanochemically Assisted Synthesis of Hexaazatriphenylenehexacarbonitrile.
Article in The Journal of organic chemistry, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.
What it found
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Who cites it
8 citing papers in PubMed.
- 1,4-Diazatriphenylene and Its Hetero-Fused Analogs: Synthesis and Applications.Molecules (Basel, Switzerland) · 2026Review
- Mechanochemical optimization and scope of triple and multiple Sonogashira couplings of triethynylbenzene for conjugated porous polymer synthesis.Scientific reports · 2026Article
- Mechanochemical Near-Ambient Synthesis of CChemSusChem · 2026Article
- Solvothermal Polymerization of Diaminomaleonitrile Reveals Optimal Green Solvents for the Production of C=N-Based Polymers.ACS omega · 2024Article
- From Inert to Catalytically Active Milling Media: Galvanostatic Coating for Direct Mechanocatalysis.Angewandte Chemie (International ed. in English) · 2022Article
- The Mechanochemical Synthesis and Activation of Carbon-Rich π-Conjugated Materials.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2022Review
- Mechanochemical Organocatalysis: Do High Enantioselectivities Contradict What We Might Expect?ChemSusChem · 2022Review
- Mechanochemically-Assisted Synthesis of Polyimides.ChemSusChem · 2022Article
Corrections and comments
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Authors and funding
4 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
1,4,5,8,9,11-hexaazatriphenylenehexacarbonitrile (HAT CN) was synthesized mechanochemically at room temperature. The coupling of hexaketocyclohexane and diaminomaleonitrile was conducted in 10 min by vibratory ball milling. The effects of milling parameters, acids, dehydrating agents, and liquid-assisted grinding were rationalized. With 67%, the yield of this mechanochemical approach exceeds that of state-of-the-art wet-chemical syntheses while being superior with respect to time-, resource-, and energy-efficiency as quantified via green metrics.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.