ArticleAngewandte Chemie (International ed. in English)2021
Mechanosynthesis of Higher-Order Cocrystals: Tuning Order, Functionality and Size in Cocrystal Design*.
Article in Angewandte Chemie (International ed. in English), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 9 papers.
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Who cites it
9 citing papers in PubMed.
- Higher-order metal-organic halogen-bonded cocrystals relying on a single supramolecular synthon.Chemical science · 2026Article
- Scalable Main Group Mechanocatalytic COAngewandte Chemie (International ed. in English) · 2025Article
- High-throughput encapsulated nanodroplet screening for accelerated co-crystal discovery.Chemical science · 2025Article
- Mechanochemistry for the Sustainable Synthesis of Organic Hole Transport Materials in Perovskite Solar Cells.Crystal growth & design · 2025Article
- Machine-Learning-Assisted Discovery of Mechanosynthesized Lead-Free Metal Halide Perovskites for the Oxidative Photocatalytic Cleavage of Alkenes.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2024Article
- Fast and scalable solvent-free access to Lappert's heavier tetrylenes E{N(SiMeChemical science · 2023Article
- Main Group Molecular Switches with Swivel Bifurcated to Trifurcated Hydrogen Bond Mode of Action.Journal of the American Chemical Society · 2023Article
- Pre-arranged building block approach for the orthogonal synthesis of an unfolded tetrameric organic-inorganic phosphazane macrocycle.Communications chemistry · 2022Article
- Mechanosynthesis of Higher-Order Cocrystals: Tuning Order, Functionality and Size in Cocrystal Design*.Angewandte Chemie (International ed. in English) · 2021Article
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Authors and funding
11 authors.
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Abstract
The ability to rationally design and predictably construct crystalline solids has been the hallmark of crystal engineering research. To date, numerous examples of multicomponent crystals comprising organic molecules have been reported. However, the crystal engineering of cocrystals comprising both organic and inorganic chemical units is still poorly understood and mostly unexplored. Here, we report a new diverse set of higher-order cocrystals (HOCs) based on the structurally versatile-yet largely unexplored-phosph(V/V)azane heterosynthon building block. The novel ternary and quaternary cocrystals reported are held together by synergistic and orthogonal intermolecular interactions. Notably, the HOCs can be readily obtained either via sequential or one-pot mechanochemical methods. Computational modelling methods reveal that the HOCs are thermodynamically driven to form and that their mechanical properties strongly depend on the composition and intermolecular forces in the crystal, offering untapped potential for optimizing material properties.
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