ArticleNanomaterials (Basel, Switzerland)2021
Facile Organometallic Synthesis of Fe-Based Nanomaterials by Hot Injection Reaction.
Article in Nanomaterials (Basel, Switzerland), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.
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2 citing papers in PubMed.
- Hyperthermia of Magnetically Soft-Soft Core-Shell Ferrite Nanoparticles.International journal of molecular sciences · 2022Article
- Synthesis, Development and Characterization of Magnetic Nanomaterials.Nanomaterials (Basel, Switzerland) · 2022Article
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5 authors.
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Abstract
Fe-based colloids with a core/shell structure consisting of metallic iron and iron oxide were synthesized by a facile hot injection reaction of iron pentacarbonyl in a multi-surfactant mixture. The size of the colloidal particles was affected by the reaction temperature and the results demonstrated that their stability against complete oxidation related to their size. The crystal structure and the morphology were identified by powder X-ray diffraction and transmission electron microscopy, while the magnetic properties were studied at room temperature with a vibrating sample magnetometer. The injection temperature plays a very crucial role and higher temperatures enhance the stability and the resistance against oxidation. For the case of injection at 315 °C, the nanoparticles had around a 10 nm mean diameter and revealed 132 emu/g. Remarkably, a stable dispersion was created due to the colloids' surface functionalization in a nonpolar solvent.
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