ArticlePolymers2021
Synthesis and Thermal Degradation Study of Polyhedral Oligomeric Silsesquioxane (POSS) Modified Phenolic Resin.
Article in Polymers, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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Who cites it
14 citing papers in PubMed, 46 citations in OpenAlex.
- Preparation of Phenolic Aerogel/Quartz Fiber Composites Modified with POSS: Low Density, High Strength and Thermal Insulation.Polymers · 2026Article
- Tailoring the Microstructure and Mechanical Properties of Phenolic Aerogels with Graphene Oxide.Gels (Basel, Switzerland) · 2025Article
- Functionalization Strategies of Non-Isocyanate Polyurethanes (NIPUs): A Systematic Review of Mechanical and Biological Advances.Polymers · 2025Review
- Effect of Metal Additives on the Structure, Morphology, and Adsorption Characteristics of the Composites: Silicon Monoxide/Phenol-Formaldehyde-Derived Carbon.International journal of molecular sciences · 2025Article
- Fabrication of Vinyl Ester-Modified Phenolic Resin Composite Coatings for the Protection of Combustible Cartridge Cases.ACS omega · 2025Article
- Study on Network Structure and Heat Resistance in Air of Boron-Modified Phenolic Resin Aerogel.Polymers · 2025Article
- Engineering Hydrogels with Enhanced Adhesive Strength Through Optimization of Poly(Ethylene Glycol) Molecular Weight.Polymers · 2025Article
- Article
- Silsesquioxane Cages under Solvent Regimen: The Influence of the Solvent on the Hydrolysis and Condensation of Alkoxysilane.Inorganic chemistry · 2024Article
- Improvement of Heat Resistance of Fluorosilicone Rubber Employing Vinyl-Functionalized POSS as a Chemical Crosslinking Agent.Polymers · 2023Article
- Article
- The Preparation and Wear Behaviors of Phenol-Formaldehyde Resin/BN Composite Coatings.Polymers · 2022Article
- Neurorobotic approaches to emulate human motor control with the integration of artificial synapse.Science advances · 2022Article
- New Ceramics Precursors Containing Si and Ge Atoms-Cubic Germasilsesquioxanes-Synthesis, Thermal Decomposition and Spectroscopic Analysis.Molecules (Basel, Switzerland) · 2022Article
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Authors and funding
5 authors at 2 institutions in 1 country.
Funding
Abstract
In this paper, a new polyhedral oligomeric silsesquioxane containing a phenol group (POSS-Phenol) is prepared through the Michael addition reaction, which is added to the synthesis of phenolic resin as a functional monomer. Infrared spectroscopy (IR) is used to demonstrate the chemistry structure of the synthesized POSS modified phenolic resin. After introducing POSS into the resole, a comprehensive study is conducted to reveal the effects of POSS on the thermal degradation of phenolic resin. First, thermal degradation behaviors of neat phenolic resin and modified phenolic resin are carried out by thermogravimetric analysis (TGA). Then, the gas volatiles from thermal degradation are investigated by thermogravimetric mass spectrometry (TG-MS). Finally, the residues after thermal degradation are characterized by X-ray diffraction (XRD). The research indicates that POSS modified phenolic resin shows a better thermal stability than neat phenolic resin, especially at high temperatures under air atmosphere. On the one hand, the introduction of the POSS group can effectively improve the release temperature of oxygen containing volatiles. On the other hand, the POSS group forms silica at high temperatures under air, which can effectively inhibit the thermal oxidation of phenolic resin and make phenolic resin show a better high-temperature oxidation resistance.
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