ArticleNature communications2021
Electrocatalytic synthesis of heterocycles from biomass-derived furfuryl alcohols.
Article in Nature communications, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.
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Who cites it
7 citing papers in PubMed, 55 citations in OpenAlex.
- Integrated Biomass Valorization: From Platform Molecules to Functional Carbon Materials for Sustainable Energy and Environmental Applications.ACS omega · 2026Review
- Boosted high-throughput D⁺ transfer from D₂O to unsaturated bonds via PdNature communications · 2025Article
- Visible-light-mediated flow protocol for Achmatowicz rearrangement.Beilstein journal of organic chemistry · 2024Article
- Article
- Microfluidic chemostatic bioreactor for high-throughput screening and sustainable co-harvesting of biomass and biodiesel in microalgae.Bioactive materials · 2023Article
- Uranium-Doped Zinc, Copper, and Nickel Oxides for Enhanced Catalytic Conversion of Furfural to Furfuryl Alcohol: A Relativistic DFT Study.Molecules (Basel, Switzerland) · 2022Article
- Efficient Electrooxidation of 5-Hydroxymethylfurfural Using Co-Doped NiAdvanced science (Weinheim, Baden-Wurttemberg, Germany) · 2022Article
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Authors and funding
7 authors at 4 institutions in 2 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
It is very attractive yet underexplored to synthesize heterocyclic moieties pertaining to biologically active molecules from biomass-based starting compounds. Herein, we report an electrocatalytic Achmatowicz reaction for the synthesis of hydropyranones from furfuryl alcohols, which can be readily produced from biomass-derived and industrially available furfural. Taking advantage of photo-induced polymerization of a bipyridyl ligand, we demonstrate the facile preparation of a heterogenized nickel electrocatalyst, which effectively drives the Achmatowicz reaction electrochemically. A suite of characterization techniques and density functional theory computations were performed to aid the understanding of the reaction mechanism. It is rationalized that the unsaturated coordination sphere of nickel sites in our electrocatalyst plays an important role at low applied potential, not only allowing the intimate interaction between the nickel center and furfuryl alcohol but also enabling the transfer of hydroxide from nickel to the bound furfuryl alcohol.
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