Evidence map›Paper›PMID 33674698›Full record

ArticleScientific reports2021

Tilting and rotational motions of silver halide crystal with diffracted X-ray blinking.

Masahiro Kuramochi, Hiroki Omata, Masaki Ishihara, Sander Ø Hanslin, Masaichiro Mizumaki, Naomi Kawamura, Hitoshi Osawa, Motohiro Suzuki, Kazuhiro Mio, Hiroshi Sekiguchi and 1 more

Abstract read
In one paragraph

Article in Scientific reports, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.

0numbers the graph read from it
0cells of the map it votes in
12citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

12 citing papers in PubMed.

  1. Article
  2. Article
  3. Article
  4. Article
  5. Review
  6. Dynamic observations of various oligomers in amyloidBiochemistry and biophysics reports · 2022
    Article
  7. Article
  8. Dynamic motions of ice-binding proteins in livingBiochemistry and biophysics reports · 2022
    Article
  9. Review
  10. Article
  11. Article
  12. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors.

Masahiro KuramochiGraduate School of Frontier Sciences, The University of Tokyo, Kashiwa, 277-8561, Japan. masahiro-kuramochi@edu.k.u-tokyo.ac.jp.ORCID https://orcid.org/0000-0003-1643-3997
Hiroki OmataGraduate School of Frontier Sciences, The University of Tokyo, Kashiwa, 277-8561, Japan.
Masaki IshiharaGraduate School of Frontier Sciences, The University of Tokyo, Kashiwa, 277-8561, Japan.
Sander Ø HanslinGraduate School of Frontier Sciences, The University of Tokyo, Kashiwa, 277-8561, Japan.
Masaichiro MizumakiCenter for Synchrotron Radiation Research, Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan.
Naomi KawamuraCenter for Synchrotron Radiation Research, Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan.
Hitoshi OsawaCenter for Synchrotron Radiation Research, Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan.
Motohiro SuzukiCenter for Synchrotron Radiation Research, Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan.
Kazuhiro MioAIST-UTokyo Advanced Operando-Measurement Technology Open Innovation Laboratory (OPERANDO-OIL), National Institute of Advanced Industrial Science and Technology (AIST), Kashiwa, 277-0882, Japan.ORCID https://orcid.org/0000-0002-1655-8231
Hiroshi SekiguchiCenter for Synchrotron Radiation Research, Japan Synchrotron Radiation Research Institute, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198, Japan.ORCID https://orcid.org/0000-0001-7590-3624
Yuji C SasakiGraduate School of Frontier Sciences, The University of Tokyo, Kashiwa, 277-8561, Japan. ycsasaki@edu.k.u-tokyo.ac.jp.ORCID https://orcid.org/0000-0003-3403-237X

Funding

Japan Society for the Promotion of Science JP20H04660JSPS Grant-in-Aid for Scientific Research on Innovative Areas "3D Active-Site Science" 26105005
6 · The paper itself

Abstract

The dynamic properties of crystalline materials are important for understanding their local environment or individual single-grain motions. A new time-resolved observation method is required for use in many fields of investigation. Here, we developed in situ diffracted X-ray blinking to monitor high-resolution diffraction patterns from single-crystal grains with a 50 ms time resolution. The diffraction spots of single grains of silver halides and silver moved in the θ and χ directions during the photolysis chemical reaction. The movements of the spots represent tilting and rotational motions. The time trajectory of the diffraction intensity reflecting those motions was analysed by using single-pixel autocorrelation function (sp-ACF). Single-pixel ACF analysis revealed significant differences in the distributions of the ACF decay constants between silver halides, suggesting that the motions of single grains are different between them. The rotational diffusion coefficients for silver halides were estimated to be accurate at the level of approximately 0.1 to 0.3 pm

Identifiers

PMID33674698
PMCPMC7935957

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.