ArticleMaterials (Basel, Switzerland)2021
Electrochemical Detection of Endosulfan Using an AONP-PANI-SWCNT Modified Glassy Carbon Electrode.
Article in Materials (Basel, Switzerland), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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4 citing papers in PubMed.
- Recent Developments in Enzyme-Free PANI-Based Electrochemical Nanosensors for Pollutant Detection in Aqueous Environments.Polymers · 2025Review
- Electrochemical Detection of Ascorbic Acid in Oranges at MWCNT-AONP Nanocomposite Fabricated Electrode.Nanomaterials (Basel, Switzerland) · 2022Article
- Electrocatalysis of Endosulfan Based on FeACS omega · 2021Article
- A Review of Nanocomposite-Modified Electrochemical Sensors for Water Quality Monitoring.Sensors (Basel, Switzerland) · 2021Review
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7 authors.
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Abstract
This report narrates the successful application of a fabricated novel sensor for the trace detection of endosulfan (EDS). The sensor was made by modifying a glassy-carbon electrode (GCE) with polyaniline (PANI), chemically synthesized antimony oxide nanoparticles (AONPs), acid-functionalized, single-walled carbon nanotubes (fSWCNTs), and finally, the AONP-PANI-SWCNT nanocomposite. The electrochemical properties of the modified electrodes regarding endosulfan detection were investigated via cyclic voltammetry (CV) and square-wave voltammetry. The current response of the electrodes to EDS followed the trend GCE-AONP-PANI-SWCNT (-510 µA) > GCE-PANI (-59 µA) > GCE-AONPs (-11.4 µA) > GCE (-5.52 µA) > GCE-fSWCNTs (-0.168 µA). The obtained results indicated that the current response obtained at the AONP-PANI-SWCNT/GCE was higher with relatively low overpotential compared to those from the other electrodes investigated. This demonstrated the superiority of the AONP-PANI-SWCNT-modified GCE. The AONP-PANI-SWCNT/GCE demonstrated good electrocatalytic activities for the electrochemical reduction of EDS. The results obtained in this study are comparable with those in other reports. The sensitivity, limit of detection (LoD), and limit of quantification (LoQ) of AONP-PANI-SWCNT/GCE towards EDS was estimated to be 0.0623 µA/µM, 6.8 µM, and 20.6 µM, respectively. Selectivity, as well as the practical application of the fabricated sensor, were explored, and the results indicated that the EDS-reduction current was reduced by only 2.0% when interfering species were present, whilst average recoveries of EDS in real samples were above 97%.
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