ArticleHeliyon2021
Remarkable enhancement of thermal stability of epoxy resin through the incorporation of mesoporous silica micro-filler.
Article in Heliyon, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 9 papers.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
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Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.
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Who cites it
9 citing papers in PubMed, 61 citations in OpenAlex.
- Solvent-free synthesis of coumarin derivatives for improved anti-corrosion and mechanical performance of primer coatings.Scientific reports · 2026Article
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- Crosslinked Gel Polymer Electrolyte from Trimethylolpropane Triglycidyl Ether by In Situ Polymerization for Lithium-Ion Batteries.Gels (Basel, Switzerland) · 2024Article
- A Comprehensive Review on the Thermal Stability Assessment of Polymers and Composites for Aeronautics and Space Applications.Polymers · 2023Review
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- Thiourea modified low molecular polyamide as a novel room temperature curing agent for epoxy resin.RSC advances · 2022Article
- New Chemically Resistant Coating Systems with Progressive Incorporation of Hazardous Waste in Polyurethane and Epoxy Matrices.Materials (Basel, Switzerland) · 2022Article
- Lab-Scale Twin-Screw Micro-Compounders as a New Rubber-Mixing Tool: 'A Comparison on EPDM/Carbon Black and EPDM/Silica Composites'.Polymers · 2021Article
Corrections and comments
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Authors and funding
10 authors at 3 institutions in 2 countries.
Funding
No grant is acknowledged in the PubMed record.
Abstract
For the first time, we incorporated mesoporous micro-silica (5 μm, pore size = 50 nm) as a filler in epoxy resin aiming to enter polymer into the pore of the silica. As expected, the thermal stability of the composite increased remarkably, followed by noteworthy thermal degradation kinetics when compared to the controlled cured epoxy resin. Composites were prepared by the direct dispersion of modified nano-silica, modified mesoporous micro-silica, unmodified mesoporous micro-silica, non-porous micro-silica, and irregular micro-silica of various pore sizes as fillers in diglycidyl ether of bisphenol-A epoxy resin via ultra-sonication and shear mixing, followed by oven-curing with 4,4-diaminodiphenyl sulfone. DSC and TGA analyses demonstrated a higher glass transition temperature (increased by 3.65-5.75 °C) and very high activation energy for thermal degradation (average increase = 46.2%) was obtained for the same unmodified silica composite compared to pure epoxy, respectively.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.