ArticleACS applied materials & interfaces2021
Pickering Emulsions Based on Wax and Halloysite Nanotubes: An Ecofriendly Protocol for the Treatment of Archeological Woods.
Article in ACS applied materials & interfaces, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 18 papers.
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Who cites it
18 citing papers in PubMed.
- Hierarchical Oil-Water-Oil Pickering Double Emulsions Stabilized by Tubular Nanoparticles.Journal of the American Chemical Society · 2026Article
- Beeswax Nanoemulsion for Consolidation and Hydrophobization of Canvases.ChemPlusChem · 2025Article
- Size-controlled assembly of phase separated protein condensates with interfacial protein cages.Nature communications · 2025Article
- Effectiveness Evaluation of Silicone Oil Emulsion In Situ Polymerization for Dehydration of Waterlogged Wooden Artifacts.Molecules (Basel, Switzerland) · 2024Article
- A ferroptosis-targeting ceria anchored halloysite as orally drug delivery system for radiation colitis therapy.Nature communications · 2023Article
- Study on the Wood Characteristics of the Chinese Ancient Ship Luoyang I.Materials (Basel, Switzerland) · 2023Article
- Characteristics of Ancient Shipwreck Wood from Huaguang Jiao No. 1 after Desalination.Materials (Basel, Switzerland) · 2023Article
- Characteristics of Ancient Ship Wood from Taicang of the Yuan Dynasty.Materials (Basel, Switzerland) · 2022Article
- Thermal and Mechanical Characterization of Yarn Samples from Flemish Tapestry of the Sixteenth Century.Molecules (Basel, Switzerland) · 2022Article
- Printable Hydrogels Based on Alginate and Halloysite Nanotubes.International journal of molecular sciences · 2022Article
- Chitosan Functionalized with Carboxyl Groups as a Recyclable Biomaterial for the Adsorption of Cu (II) and Zn (II) Ions in Aqueous Media.International journal of molecular sciences · 2022Article
- Barrier Dispersion-Based Coatings Containing Natural and Paraffin Waxes.Molecules (Basel, Switzerland) · 2022Article
- Recent Developments in the Application of Inorganic Nanomaterials and Nanosystems for the Protection of Cultural Heritage Organic Artifacts.Nanomaterials (Basel, Switzerland) · 2022Review
- Conversion of Organic Dyes into Pigments: Extraction of Flavonoids from Blackberries (Molecules (Basel, Switzerland) · 2021Article
- The Viscoelastic Behaviour of Waterlogged Archaeological Wood Treated with Methyltrimethoxysilane.Materials (Basel, Switzerland) · 2021Article
- Understanding the Effects of Crosslinking and Reinforcement Agents on the Performance and Durability of Biopolymer Films for Cultural Heritage Protection.Molecules (Basel, Switzerland) · 2021Article
- Effect of Surfactant Molecular Structure on Emulsion Stability Investigated by Interfacial Dilatational Rheology.Polymers · 2021Article
- Sepiolite-Hydrogels: Synthesis by Ultrasound Irradiation and Their Use for the Preparation of Functional Clay-Based Nanoarchitectured Materials.Frontiers in chemistry · 2021Article
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Authors and funding
5 authors.
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Abstract
A novel green protocol for the consolidation and protection of waterlogged archeological woods with wax microparticles has been designed. First, we focused on the development of halloysite nanotubes (HNTs) based Pickering emulsions using wax as the inner phase of the oil-in-water droplets. The optimization of the preparation strategy was supported by both optical microscopy and scanning electron microscopy, which allowed us to show the morphological features of the prepared hybrid systems and their structural properties, i.e., the distribution of the clay at the interface. Also, the dependence of the overall dimensions of the prepared systems on the halloysite content was demonstrated. Microdifferential scanning calorimetry (μ-DSC) was conducted in order to assess whether the thermal properties of the wax are affected after its interaction with HNTs. Then, the Pickering emulsions were employed for the treatment of waterlogged wooden samples. Compared to the archeological woods treated with pure wax, the addition of nanotubes induced a remarkable improvement in the mechanical performance in terms of stiffness and flexural strength. The proposed protocol is environmentally friendly since water is the only solvent used throughout the entire procedure, even if wax is vehiculated into the pores at room temperature. As a consequence, the design of wax/halloysite Pickering emulsions represents a promising strategy for the preservation of wooden artworks, and it has a great potential to be scaled up, thus becoming also exploitable for the treatments of shipwrecks of large size.
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