Supramolecular Solvent-Based Microextraction of Selected Anticonvulsant and Nonsteroidal Anti-Inflammatory Drugs from Sediment Samples.

Sylwia Bajkacz, Paulina Adamczewska, Klaudia Kokoszka, Elżbieta Kycia-Słocka, Adam Sochacki, Ewa Felis

Open access · goldAbstract read

In one paragraph

Article in Molecules (Basel, Switzerland), 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it

0cells of the map it votes in

1citing papers in PubMed

0.4field-weighted citation impact, top 45% of its field

1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 6 citations in OpenAlex.

Ultrasound assisted supramolecular liquid phase microextraction procedure for Sudan I at trace level in environmental samples.Turkish journal of chemistry · 2021
Article

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 1 institution in 2 countries.

Sylwia BajkaczDepartment of Inorganic Chemistry, Analytical Chemistry and Electrochemistry, Faculty of Chemistry, Silesian University of Technology, B. Krzywoustego 6 St., 44-100 Gliwice, Poland.

Paulina AdamczewskaDepartment of Inorganic Chemistry, Analytical Chemistry and Electrochemistry, Faculty of Chemistry, Silesian University of Technology, B. Krzywoustego 6 St., 44-100 Gliwice, Poland.

Klaudia KokoszkaDepartment of Inorganic Chemistry, Analytical Chemistry and Electrochemistry, Faculty of Chemistry, Silesian University of Technology, B. Krzywoustego 6 St., 44-100 Gliwice, Poland.ORCID 0000-0002-6823-241X

Elżbieta Kycia-SłockaDepartment of Inorganic Chemistry, Analytical Chemistry and Electrochemistry, Faculty of Chemistry, Silesian University of Technology, B. Krzywoustego 6 St., 44-100 Gliwice, Poland.

Adam SochackiEnvironmental Biotechnology Department, Faculty of Power and Environmental Engineering, Silesian University of Technology, Akademicka 2 St., 44-100 Gliwice, Poland.ORCID 0000-0001-8803-005X

Ewa FelisEnvironmental Biotechnology Department, Faculty of Power and Environmental Engineering, Silesian University of Technology, Akademicka 2 St., 44-100 Gliwice, Poland.

Silesian University of Technology · PL

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The increase in the production and consumption of pharmaceuticals increases their presence in the global environment, which may result in direct threats to living organisms. For this reason, there is a need for new methods to analyze drugs in environmental samples. Here, a new procedure for separating and determining selected drugs (diclofenac, ibuprofen, and carbamazepine) from bottom sediment and water samples was developed. Drugs were determined by ultra-high performance liquid chromatography coupled with an ultraviolet detector (UHPLC-UV). In this work, a universal and single-step sample treatment, based on supramolecular solvents (SUPRAS), was proposed to isolate selected anticonvulsants and nonsteroidal anti-inflammatory drugs (NSAIDs) from sediment samples. The following parameters were experimentally selected: composition of the supramolecular solvent (composition THF:H

Indexed as

AnticonvulsantsAnti-Inflammatory Agents, Non-SteroidalLimit of DetectionLiquid Phase MicroextractionPharmaceutical PreparationsSolventsWater Pollutants, ChemicalAnticonvulsantsAnti-Inflammatory Agents, Non-SteroidalPharmaceutical PreparationsSolventsWater Pollutants, Chemicalliquid chromatographymicropollutantsSpeedisksupramolecular solvent-based microextraction

Identifiers

PMID33271858

DOI10.3390/molecules25235671

PMCPMC7729498

OpenAlexW3108757347

What OpenQuestion holds

Textmetadata

LicenceCC BY

Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.