ArticleChemistryOpen2020
Mechanism of Bi-Ni Phase Formation in a Microwave-Assisted Polyol Process.
Article in ChemistryOpen, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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4 citing papers in PubMed, 16 citations in OpenAlex.
- Bimetallic Bismuth-Based Nanoparticles From Pseudo-Tetrahedral Zintl Anions.Small (Weinheim an der Bergstrasse, Germany) · 2026Article
- Microwave-Assisted Synthesis of IrNi Electrocatalysts for the Oxygen Evolution Reaction in Acidic Electrolyte.ChemistryOpen · 2025Article
- In situ Investigations of the Formation Mechanism of Metastable γ-BiPd Nanoparticles in Polyol Reductions.ChemistryOpen · 2024Article
- Mechanism of Bi-Ni Phase Formation in a Microwave-Assisted Polyol Process.ChemistryOpen · 2020Article
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4 authors at 3 institutions in 1 country.
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Abstract
Typically, intermetallic phases are obtained in solid-state reactions or crystallization from melts, which are highly energy and time consuming. The polyol process takes advantage of low temperatures and short reaction times using easily obtainable starting materials. The formation mechanism of these intermetallic particles has received little attention so far, even though a deeper understanding should allow for better synthesis planning. In this study, we therefore investigated the formation of BiNi particles in ethylene glycol in a microwave-assisted polyol process mechanistically. The coordination behavior in solution was analyzed using HPLC-MS and UV-Vis. Tracking the reaction with PXRD measurements, FT-IR spectroscopy and HR-TEM revealed a successive reduction of Bi
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