Evidence map›Paper›PMID 33129618›Full record

ArticleFood chemistry2021

Determination of glyphosate and AMPA in oat products for the selection of candidate reference materials.

Justine M Cruz, Jacolin A Murray

Open access · greenAbstract read
In one paragraph

Article in Food chemistry, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 9 papers.

0numbers the graph read from it
0cells of the map it votes in
9citing papers in PubMed
0.4field-weighted citation impact, top 44% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

9 citing papers in PubMed, 20 citations in OpenAlex.

  1. Residues of Desiccant Herbicides in Sesame Seeds (Journal of agricultural and food chemistry · 2026
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

2 authors at 1 institution in 1 country.

Justine M CruzU.S. National Institute of Standards and Technology, Chemical Sciences Division, 100 Bureau Drive, Gaithersburg, MD 20899-8392, USA.
Jacolin A MurrayU.S. National Institute of Standards and Technology, Chemical Sciences Division, 100 Bureau Drive, Gaithersburg, MD 20899-8392, USA. Electronic address: jacolin.murray@nist.gov.
National Institute of Standards and Technology · US

Funding

Intramural NIST DOC 9999-NIST
6 · The paper itself

Abstract

The use of reference materials (RMs) is critical for validating and testing the accuracy of analytical protocols. The National Institute of Standards and Technology (NIST) is in initial stages of developing a glyphosate in oats RM. The first aim of this study was to optimize and validate a robust method for the extraction and analysis of glyphosate and aminomethylphosphonic acid (AMPA). The optimized method was used to screen thirteen commercially available oat products to identify candidate RMs. Glyphosate was detected in all samples, with the highest glyphosate mass fraction of 1100 ng/g; lower levels were measured in grains from organic agriculture. AMPA was quantified in nine samples up to 40 ng/g. The findings of this study led to the identification of candidate RMs, with "high" and "low" glyphosate levels. A preliminary stability study determined that glyphosate is stable in oat material at room temperature for six months.

Indexed as

AvenaFood AnalysisGlycineGlyphosateOrganophosphonatesReference Standardsaminomethylphosphonic acid (AMPA)GlycineGlyphosateOrganophosphonates(Aminomethyl) phosphonic Acid-(13)C,(15)N (PubChem CID: 76974379)(Aminomethyl)phosphonic acid-FMOC (PubChem CID: 15339930)(Aminomethyl)phosphonic acid (PubChem CID: 14017)AMPAGlyphosateGlyphosate-(13)C2,(15)N (PubChem CID: 46780452)Glyphosate-FMOC (PubChem CID: 101243275)Glyphosate (PubChem CID: 3496)Liquid chromatography tandem mass spectrometryOat-based cerealsOatmealOatsReference material

Identifiers

PMID33129618
PMCPMC8207808
OpenAlexW3087894525

What OpenQuestion holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.