ArticleAnalytical and bioanalytical chemistry2021
Methanol-based extraction protocol for insoluble and moderately water-soluble nanoparticles in plants to enable characterization by single particle ICP-MS.
Article in Analytical and bioanalytical chemistry, 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 11 papers.
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11 citing papers in PubMed, 27 citations in OpenAlex.
- Evaluation of extraction capabilities of protease, proteinase K, and TMAH for nanoparticle characterization in biological CRMs by spICP-MS.Analytical and bioanalytical chemistry · 2026Article
- Convenient colorimetric approach to quantify CuO NPs in water using only a smartphone and cellulose paper with an immobilised chemosensor.Mikrochimica acta · 2025Article
- SI-traceable characterisation of the first reference material for nanoparticle number concentration in suspension to support regulatory compliance.Analytical and bioanalytical chemistry · 2025Article
- Nano Spirulina platensis countered cisplatin-induced repro-toxicity by reversing the expression of altered steroid hormones and downregulation of the StAR gene.Naunyn-Schmiedeberg's archives of pharmacology · 2025Article
- Advances and Challenges in Tracking Interactions Between Plants and Metal-Based Nanoparticles.Nanomaterials (Basel, Switzerland) · 2024Review
- Zinc oxide nanoparticles cooperate with the phyllosphere to promote grain yield and nutritional quality of rice under heatwave stress.Proceedings of the National Academy of Sciences of the United States of America · 2024Article
- Evaluation of the effect of nanoparticles on the cultivation of edible plants by ICP-MS: a review.Analytical and bioanalytical chemistry · 2024Review
- Effect of a Zinc Phosphate Shell on the Uptake and Translocation of Foliarly Applied ZnO Nanoparticles in Pepper Plants (Environmental science & technology · 2024Article
- Application of Single Particle ICP-MS for the Determination of Inorganic Nanoparticles in Food Additives and Food: A Short Review.Nanomaterials (Basel, Switzerland) · 2023Review
- Analysis of Silver Nanoparticles in Ground Beef by Single Particle Inductively Coupled Plasma Mass Spectrometry (SP-ICP-MS).Molecules (Basel, Switzerland) · 2023Article
- Determination of metallic nanoparticles in biological samples by single particle ICP-MS: a systematic review from sample collection to analysis.Environmental science. Nano · 2022Review
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Authors and funding
7 authors at 2 institutions in 2 countries.
Funding
Abstract
The detection and characterization of soluble metal nanoparticles in plant tissues are an analytical challenge, though a scientific necessity for regulating nano-enabled agrichemicals. The efficacy of two extraction methods to prepare plant samples for analysis by single particle ICP-MS, an analytical method enabling both size determination and quantification of nanoparticles (NP), was assessed. A standard enzyme-based extraction was compared to a newly developed methanol-based approach. Au, CuO, and ZnO NPs were extracted from three different plant leaf materials (lettuce, corn, and kale) selected for their agricultural relevance and differing characteristics. The enzyme-based approach was found to be unsuitable because of changes in the recovered NP size distribution of CuO NP. The MeOH-based extraction allowed reproducible extraction of the particle size distribution (PSD) without major alteration caused by the extraction. The type of leaf tissue did not significantly affect the recovered PSD. Total metal losses during the extraction process were largely due to the filtration step prior to analysis by spICP-MS, though this did not significantly affect PSD recovery. The methanol extraction worked with the three different NPs and plants tested and is suitable for studying the fate of labile metal-based nano-enabled agrichemicals.
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