ArticleMaterials (Basel, Switzerland)2020
Self-Organized Anodic Oxides on Titanium Alloys Prepared from Glycol- and Glycerol-Based Electrolytes.
Article in Materials (Basel, Switzerland), 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.
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6 citing papers in PubMed, 30 citations in OpenAlex.
- Current Density Optimization for SERS Substrates Using Galvanostatically Anodized TiOMaterials (Basel, Switzerland) · 2025Article
- Porous-Wall Titania Nanotube Array Layers: Preparation and Photocatalytic Response.Nanomaterials (Basel, Switzerland) · 2023Article
- Nitrilotriacetic Acid Improves Plasma Electrolytic Oxidation of Titanium for Biomedical Applications.ACS applied materials & interfaces · 2023Article
- Modification of Anodic Titanium Oxide Bandgap Energy by Incorporation of Tungsten, Molybdenum, and Manganese In Situ during Anodization.Materials (Basel, Switzerland) · 2023Article
- Production, Characterization and Application of Oxide Nanotubes on Ti-6Al-7Nb Alloy as a Potential Drug Carrier.Materials (Basel, Switzerland) · 2021Article
- Anodic TiONanomaterials (Basel, Switzerland) · 2021Review
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5 authors at 2 institutions in 2 countries.
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Abstract
The anodization of commercially pure Ti alloy (99.5 wt %) and two biomedical titanium alloys, Ti6Al7Nb and Ti6Al4V, was performed, and the resulting anodic oxides were studied. The biomedical alloys were made by Laser Engineered Net Shaping. The glycol-based and glycerol-based electrolytes with 0.3 M ammonium fluoride and 2 wt % of deionized water content were tested. It was found that electrolyte type as well as the chemical composition of the base substrate affected the final morphology and chemical composition of the anodic oxide formed. A higher current density, ionic mobility, and oxide growth rate were obtained in glycol-based electrolyte as compared to those obtained in glycerol-based electrolyte for all tested alloys. A self-organized nanotubular and nanoporous morphology of the anodic oxide in both types of electrolyte was obtained. In each electrolyte, the alloy susceptibility to oxidation increased in the following order: Ti6Al4V < Ti 99.5% < Ti6Al7Nb, which can be correlated to the oxidation susceptibility of the base titanium alloy. It was observed that the more impurities/alloying elements in the substrate, the lower the pore diameters of anodic oxide. There was a higher observed incorporation of electrolyte species into the anodic oxide matrix in the glycerol-based electrolyte compared with that in glycol-based electrolyte.
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