Evidence map›Paper›PMID 32973262›Full record

ArticleScientific reports2020

Synthesis conditions influencing formation of MAPbBr

Anna Jancik Prochazkova, Markus Clark Scharber, Cigdem Yumusak, Ján Jančík, Jiří Másilko, Oliver Brüggemann, Martin Weiter, Niyazi Serdar Sariciftci, Jozef Krajcovic, Yolanda Salinas and 1 more

Open access · goldAbstract read
In one paragraph

Article in Scientific reports, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.

0numbers the graph read from it
0cells of the map it votes in
5citing papers in PubMed
2.6field-weighted citation impact, top 10% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

5 citing papers in PubMed, 48 citations in OpenAlex.

  1. Article
  2. Synthesis of trypsin-protected CsPbClMikrochimica acta · 2025
    Article
  3. Colloidal Synthesis of (PbBrCrystal growth & design · 2024
    Article
  4. Article
  5. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors at 2 institutions in 2 countries.

Anna Jancik ProchazkovaLinz Institute for Organic Solar Cells (LIOS), Physical Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria. anna@roproch.cz.
Markus Clark ScharberLinz Institute for Organic Solar Cells (LIOS), Physical Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Cigdem YumusakLinz Institute for Organic Solar Cells (LIOS), Physical Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Ján JančíkFaculty of Chemistry, Materials Research Centre, Brno University of Technology, Purkyňova 118, 61200, Brno, Czech Republic.
Jiří MásilkoFaculty of Chemistry, Materials Research Centre, Brno University of Technology, Purkyňova 118, 61200, Brno, Czech Republic.
Oliver BrüggemannInstitute of Polymer Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Martin WeiterFaculty of Chemistry, Materials Research Centre, Brno University of Technology, Purkyňova 118, 61200, Brno, Czech Republic.
Niyazi Serdar SariciftciLinz Institute for Organic Solar Cells (LIOS), Physical Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Jozef KrajcovicFaculty of Chemistry, Materials Research Centre, Brno University of Technology, Purkyňova 118, 61200, Brno, Czech Republic.
Yolanda SalinasInstitute of Polymer Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Alexander KovalenkoLinz Institute for Organic Solar Cells (LIOS), Physical Chemistry, Johannes Kepler University Linz, Altenberger Straße 69, 4040, Linz, Austria.
Johannes Kepler University of Linz · ATBrno University of Technology · CZ

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This work reports on an optimized procedure to synthesize methylammonium bromide perovskite nanoparticles. The ligand-assisted precipitation synthetic pathway for preparing nanoparticles is a cost-effective and promising method due to its ease of scalability, affordable equipment requirements and convenient operational temperatures. Nevertheless, there are several parameters that influence the resulting optical properties of the final nanomaterials. Here, the influence of the choice of solvent system, capping agents, temperature during precipitation and ratios of precursor chemicals is described, among other factors. Moreover, the colloidal stability and stability of the precursor solution is studied. All of the above-mentioned parameters were observed to strongly affect the resulting optical properties of the colloidal solutions. Various solvents, dispersion media, and selection of capping agents affected the formation of the perovskite structure, and thus qualitative and quantitative optimization of the synthetic procedure conditions resulted in nanoparticles of different dimensions and optical properties. The emission maxima of the nanoparticles were in the 508-519 nm range due to quantum confinement, as confirmed by transmission electron microscopy. This detailed study allows the selection of the best optimal conditions when using the ligand-assisted precipitation method as a powerful tool to fine-tune nanostructured perovskite features targeted for specific applications.

Identifiers

PMID32973262
PMCPMC7518261
OpenAlexW3088738423

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.