Evidence map›Paper›PMID 32897435›Full record

ArticleMikrochimica acta2020

In situ formed zinc oxide/graphitic carbon nitride nanohybrid for the electrochemical determination of 4-nitrophenol.

Kizhepat Shamsa, Peter Selvaraj Mary Rajaitha, Selvaraj Vinoth, Chinnan Murugan, Perumal Rameshkumar, Alagarsamy Pandikumar

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In one paragraph

Article in Mikrochimica acta, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
1.8field-weighted citation impact, top 15% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

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3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 32 citations in OpenAlex.

  1. Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 2 institutions in 1 country.

Kizhepat ShamsaElectro Organic and Materials Electrochemistry (EME) Division, CSIR-Central Electrochemical Research Institute, Karaikudi, Tamil Nadu, 630 003, India.
Peter Selvaraj Mary RajaithaElectro Organic and Materials Electrochemistry (EME) Division, CSIR-Central Electrochemical Research Institute, Karaikudi, Tamil Nadu, 630 003, India.
Selvaraj VinothElectro Organic and Materials Electrochemistry (EME) Division, CSIR-Central Electrochemical Research Institute, Karaikudi, Tamil Nadu, 630 003, India.
Chinnan MuruganElectro Organic and Materials Electrochemistry (EME) Division, CSIR-Central Electrochemical Research Institute, Karaikudi, Tamil Nadu, 630 003, India.
Perumal RameshkumarDepartment of Chemistry, School of Advanced Sciences, Kalasalingam Academy of Research and Education, Krishnankoil, Tamil Nadu, 626 126, India. rameshkumar.p@klu.ac.in.
Alagarsamy PandikumarElectro Organic and Materials Electrochemistry (EME) Division, CSIR-Central Electrochemical Research Institute, Karaikudi, Tamil Nadu, 630 003, India. pandikumarinbox@gmail.com.ORCID http://orcid.org/0000-0002-8804-5195
Central Electrochemical Research Institute · INKalasalingam Academy of Research and Education · IN

Funding

Science and Engineering Research Board ECR/2017/001758
6 · The paper itself

Abstract

The electrochemical determination of 4-nitrophenol using a nanohybrid consisting of glassy carbon (GC) and zinc oxide/graphitic carbon nitride (ZnO/g-CN nanosheet), is described. The ZnO/g-CN nanohybrid was in situ synthesized by chemical method and well characterized using absorption spectroscopy, X-ray diffraction, X-ray photoelectron spectroscopy and transmission electron microscopic analysis. It was observed that the nanosized ZnO particles were present inside the sheet-like g-CN nanostructure. The nanohybrid-modified electrode showed an enhanced electrocatalytic response for 4-nitrophenol reduction compared with the bare GC electrode. The assay exhibited linear ranges of 13.4-100 μM and 100-1000 μM for 4-NP determination. The limit of detection and limit of quantification were 4.0 and 13.4 μM, respectively, at the working potential of - 0.85 V. An appreciable precision was found towards the stability of the assay in the determination. It provides selectivity against inorganic and organic substances such as calcium chloride, potassium chloride, nitrobenzene, uric acid, 1-chloro,2,4-dinitrobenzene, 1-bromo,2-nitrobenzene and 1-iodo,2-nitrobenzene. The practical applicability of the assay was also checked in the analysis of real water samples and satisfactory recovery of 4-NP was found. Schematic representation of the synthesis of zinc oxide (ZnO) nanostructures incorporated graphitic carbon nitride nanosheets (g-C

Indexed as

2D materials4-NitrophenolElectrochemical assayElectrochemical sensorGraphitic carbon nitrideMetal oxide nanostructuresModified electrodeNanohybridNitroaromaticsZinc oxide

Identifiers

PMID32897435
OpenAlexW3084281498

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.