Evidence map›Paper›PMID 32876620›Full record

ArticleJournal of synchrotron radiation2020

Combining Laue diffraction with Bragg coherent diffraction imaging at 34-ID-C.

Anastasios Pateras, Ross Harder, Wonsuk Cha, Jonathan G Gigax, J Kevin Baldwin, Jon Tischler, Ruqing Xu, Wenjun Liu, Mark J Erdmann, Robert Kalt and 3 more

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of synchrotron radiation, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

13 authors.

Anastasios PaterasMaterials Science and Technology Division, Los Alamos National Laboratory, PO Box 1663, Los Alamos, NM 87545, USA.ORCID 0000-0001-5642-7669
Ross HarderAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Wonsuk ChaAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.ORCID 0000-0001-8888-4258
Jonathan G GigaxCenter for Integrated Nanotechnologies, Los Alamos National Laboratory, PO Box 1663, Los Alamos, NM 87545, USA.
J Kevin BaldwinCenter for Integrated Nanotechnologies, Los Alamos National Laboratory, PO Box 1663, Los Alamos, NM 87545, USA.
Jon TischlerAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Ruqing XuAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Wenjun LiuAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Mark J ErdmannAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Robert KaltAdvanced Photon Source, Argonne National Laboratory, Lemont, IL 60439, USA.
Richard L SandbergDepartment of Physics and Astronomy, Brigham Young University, Provo, UT 84602, USA.
Saryu FensinMaterials Science and Technology Division, Los Alamos National Laboratory, PO Box 1663, Los Alamos, NM 87545, USA.
Reeju PokharelMaterials Science and Technology Division, Los Alamos National Laboratory, PO Box 1663, Los Alamos, NM 87545, USA.

Funding

This work was supported by the US Department of Energy through Los Alamos National Laboratory. Los Alamos National Laboratory (LANL) is operated by Triad National Security, LLC, for the National Nuclear Security Administration of the US Department of Energy (Contract No. 89233218CNA000001). AP, JGG, JKB, SF and RP acknowledge funding from LANL's Director's Initiative LDRD Project #20190643DI. LANL's Science Campaign (C2) Program funding for commissioning of the double bounce monochromator is also acknowledged. This research used resources of the Advanced Photon Source, a US Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357. 20190643DIThis work was supported by the US Department of Energy through Los Alamos National Laboratory. Los Alamos National Laboratory (LANL) is operated by Triad National Security, LLC, for the National Nuclear Security Administration of the US Department of Energy (Contract No. 89233218CNA000001). AP, JGG, JKB, SF and RP acknowledge funding from LANL's Director's Initiative LDRD Project #20190643DI. LANL's Science Campaign (C2) Program funding for commissioning of the double bounce monochromator is also acknowledged. This research used resources of the Advanced Photon Source, a US Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357. 89233218CNA000001This work was supported by the US Department of Energy through Los Alamos National Laboratory. Los Alamos National Laboratory (LANL) is operated by Triad National Security, LLC, for the National Nuclear Security Administration of the US Department of Energy (Contract No. 89233218CNA000001). AP, JGG, JKB, SF and RP acknowledge funding from LANL's Director's Initiative LDRD Project #20190643DI. LANL's Science Campaign (C2) Program funding for commissioning of the double bounce monochromator is also acknowledged. This research used resources of the Advanced Photon Source, a US Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357. DE-AC02-06CH11357
6 · The paper itself

Abstract

Measurement modalities in Bragg coherent diffraction imaging (BCDI) rely on finding a signal from a single nanoscale crystal object which satisfies the Bragg condition among a large number of arbitrarily oriented nanocrystals. However, even when the signal from a single Bragg reflection with (hkl) Miller indices is found, the crystallographic axes on the retrieved three-dimensional (3D) image of the crystal remain unknown, and thus localizing in reciprocal space other Bragg reflections becomes time-consuming or requires good knowledge of the orientation of the crystal. Here, the commissioning of a movable double-bounce Si (111) monochromator at the 34-ID-C endstation of the Advanced Photon Source is reported, which aims at delivering multi-reflection BCDI as a standard tool in a single beamline instrument. The new instrument enables, through rapid switching from monochromatic to broadband (pink) beam, the use of Laue diffraction to determine crystal orientation. With a proper orientation matrix determined for the lattice, one can measure coherent diffraction patterns near multiple Bragg peaks, thus providing sufficient information to image the full strain tensor in 3D. The design, concept of operation, the developed procedures for indexing Laue patterns, and automated measuring of Bragg coherent diffraction data from multiple reflections of the same nanocrystal are discussed.

Indexed as

BCDIBragg diffractionLaue diffractionstrain imaging

Identifiers

PMID32876620
PMCPMC7467351

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.