ArticleJournal of synchrotron radiation2020
Fast operando X-ray pair distribution function using the DRIX electrochemical cell.
Article in Journal of synchrotron radiation, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 13 papers.
What it found
Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.
The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
The trial behind it
Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.
Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.
Who cites it
13 citing papers in PubMed.
- Sample environment forJournal of applied crystallography · 2026Article
- Revisiting potassium intercalation in graphite: anEES batteries · 2026Article
- Distinguishing isotropic and anisotropic signals for X-ray total scattering using machine learning.Acta crystallographica. Section A, Foundations and advances · 2025Article
- Best practices for in-situ and operando techniques within electrocatalytic systems.Nature communications · 2025Review
- The AUREX cell: a versatileJournal of applied crystallography · 2024Article
- Electrochemical cell for synchrotron nuclear resonance techniques.Journal of synchrotron radiation · 2024Article
- Review
- Monitoring surface dynamics of electrodes during electrocatalysis using in situ synchrotron FTIR spectroscopy.Journal of synchrotron radiation · 2023Article
- Total scattering measurements at the Australian Synchrotron Powder Diffraction beamline: capabilities and limitations.Journal of synchrotron radiation · 2023Article
- Synchrotron radiation basedChemical science · 2023Review
- Structural Analysis of Molecular Materials Using the Pair Distribution Function.Chemical reviews · 2022Review
- Recovering local structure information from high-pressure total scattering experiments.Journal of applied crystallography · 2021Article
- Bridging Structural Inhomogeneity to Functionality: Pair Distribution Function Methods for Functional Materials Development.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2021Review
Corrections and comments
PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.
Authors and funding
8 authors.
Funding
Abstract
In situ electrochemical cycling combined with total scattering measurements can provide valuable structural information on crystalline, semi-crystalline and amorphous phases present during (dis)charging of batteries. In situ measurements are particularly challenging for total scattering experiments due to the requirement for low, constant and reproducible backgrounds. Poor cell design can introduce artefacts into the total scattering data or cause inhomogeneous electrochemical cycling, leading to poor data quality or misleading results. This work presents a new cell design optimized to provide good electrochemical performance while performing bulk multi-scale characterizations based on total scattering and pair distribution function methods, and with potential for techniques such as X-ray Raman spectroscopy. As an example, the structural changes of a nanostructured high-capacity cathode with a disordered rock-salt structure and composition Li
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.