Evidence map›Paper›PMID 32860534›Full record

ArticleMikrochimica acta2020

In-tube stir bar sorptive extraction based on 3-aminopropyl triethoxysilane surface-modified Ce-doped ZnAl layered double hydroxide thin film for determination of nonsteroidal anti-inflammatory drugs in saliva samples.

Mahsa Torabi Mirzaee, Shahram Seidi, Yasaman Razeghi, Mahshid Manouchehri, Maryam Shanehsaz

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Article in Mikrochimica acta, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Mahsa Torabi MirzaeeDepartment of Analytical Chemistry, Faculty of Chemistry, K.N. Toosi University of Technology, P.O. Box 16315-1618, Tehran, Iran.
Shahram SeidiDepartment of Analytical Chemistry, Faculty of Chemistry, K.N. Toosi University of Technology, P.O. Box 16315-1618, Tehran, Iran. s.seidi@kntu.ac.ir.
Yasaman RazeghiDepartment of Analytical Chemistry, Faculty of Chemistry, K.N. Toosi University of Technology, P.O. Box 16315-1618, Tehran, Iran.
Mahshid ManouchehriDepartment of Analytical Chemistry, Faculty of Chemistry, K.N. Toosi University of Technology, P.O. Box 16315-1618, Tehran, Iran.
Maryam ShanehsazAnalytical Chemistry Research Laboratory, Mobin Shimi Azma Company, Tehran, Iran.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A thin-film based on 3-aminopropyl triethoxysilane surface-modified Ce-doped zinc-aluminum layered double hydroxide was synthesized on the inner surface of an aluminum tube. It has been applied to in-tube stir bar sorptive extraction of nonsteroidal anti-inflammatory drugs in saliva samples followed by high-performance liquid chromatography. The sorbent was characterized by scanning electron microscopy, X-ray diffraction, Fourier-transform infrared spectroscopy, energy-dispersive X-ray spectroscopy, and elemental mapping. The extraction parameters including sample pH (4.2), extraction time (10 min), stirring speed (800 rpm), type of eluent (acidified tetrahydrofuran), eluent volume (100 μL), and desorption time (6 min) were thoroughly optimized. Under the optimum conditions, limits of detection were found to be less than 5.0 ng mL

Indexed as

AdsorptionAluminumAnti-Inflammatory Agents, Non-SteroidalCeriumChromatography, High Pressure LiquidHydroxidesLimit of DetectionPropylaminesReproducibility of ResultsSalivaSilanesSolid Phase ExtractionSpectrophotometry, UltravioletZincAluminumamino-propyl-triethoxysilaneAnti-Inflammatory Agents, Non-SteroidalCeriumHydroxidesPropylaminesSilanesZincBiological fluidsDiclofenacMefenamic acidMicroextractionNanosorbentNaproxenTrace analysis

Identifiers

PMID32860534

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