ArticleACS applied materials & interfaces2020
Operando Electrochemical Atomic Force Microscopy of Solid-Electrolyte Interphase Formation on Graphite Anodes: The Evolution of SEI Morphology and Mechanical Properties.
Article in ACS applied materials & interfaces, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 22 papers.
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Who cites it
22 citing papers in PubMed.
- Atomic force nanorheology forFaraday discussions · 2026Article
- Modulated electrochemical force microscopy: Investigation of sodium-ion transport at hard carbon composite anodes.Journal of microscopy · 2026Article
- Atomic Force Microscopy for Cross-Disciplinary Materials Research.Small methods · 2025Review
- Saturating the Matrix: Nanocomposite Solution-Processed Sodium Aluminophosphate Solid Electrolytes.ACS applied energy materials · 2025Article
- Unlocking Solid Polymer Electrolytes: Advancing Materials through Characterization-Driven Insights.JACS Au · 2025Review
- Structural Evolution of Silicon Nitride Anodes during Electrochemical Lithiation.ACS electrochemistry · 2025Article
- Recent advances in characterization of rechargeable battery materialsJournal of materials chemistry. A · 2025Article
- Electrochemical Atomic Force Microscopy of Black Phosphorus Composite Anodes: Electrode Destabilization and Degradation Mechanisms in Alkali-Ion Batteries.ACS applied materials & interfaces · 2024Article
- Electrolyte-Electrocatalyst Interfacial Effects of Polymeric Materials for Tandem COACS applied materials & interfaces · 2024Article
- The Influence of Cathode Degradation Products on the Anode Interface in Lithium-Ion Batteries.ACS nano · 2024Article
- Article
- Operando spectral imaging of the lithium ion battery's solid-electrolyte interphase.Science advances · 2023Article
- The role of ion solvation in lithium mediated nitrogen reduction.Journal of materials chemistry. A · 2023Article
- An Integrated, Exchangeable Three-Electrode Electrochemical Setup for AFM-Based Scanning Electrochemical Microscopy.Sensors (Basel, Switzerland) · 2023Article
- Article
- Article
- Nanoarchitecture factors of solid electrolyte interphase formation via 3D nano-rheology microscopy and surface force-distance spectroscopy.Nature communications · 2023Article
- Near ambient NNature reviews. Chemistry · 2023Review
- Sodium Dual-Ion Batteries with Concentrated Electrolytes.ChemSusChem · 2023Article
- Nanoscale Visualization of the Electron Conduction Channel in the SiO/Graphite Composite Anode.ACS applied materials & interfaces · 2022Article
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Authors and funding
6 authors.
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No grant is acknowledged in the PubMed record.
Abstract
Understanding and ultimately controlling the properties of the solid-electrolyte interphase (SEI) layer at the graphite anode/liquid electrolyte boundary are of great significance for maximizing the performance and lifetime of lithium-ion batteries (LIBs). However, comprehensive in situ monitoring of SEI formation and evolution, alongside measurement of the corresponding mechanical properties, is challenging due to the limitations of the characterization techniques commonly used. This work provides a new insight into SEI formation during the first lithiation and delithiation of graphite battery anodes using operando electrochemical atomic force microscopy (EC-AFM). Highly oriented pyrolytic graphite (HOPG) is investigated first as a model system, exhibiting unique morphological and nanomechanical behavior dependent on the various electrolytes and commercially relevant additives used. Then, to validate these findings with respect to real-world battery electrodes, operando EC-AFM of individual graphite particles like those in commercial systems are studied. Vinylene carbonate (VC) and fluoroethylene carbonate (FEC) are shown to be effective additives to enhance SEI layer stability in 1 M LiPF
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