ArticleEnvironmental science and pollution research international2020
The quantification of bisphenols and their analogues in wastewaters and surface water by an improved solid-phase extraction gas chromatography/mass spectrometry method.
Article in Environmental science and pollution research international, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 9 papers.
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Who cites it
9 citing papers in PubMed, 56 citations in OpenAlex.
- Adsorptive removal of losartan, bisphenol A, and triclosan in aqueous solutions using a graphene oxide-enhanced MOF-Zn composite.Environmental science and pollution research international · 2025Article
- Effects of Acute and Developmental Exposure to Bisphenol S on Chinese Medaka (Journal of xenobiotics · 2024Article
- Relationship between Eating Habits and 4-Nonylphenol Concentration in Breast Milk of Women in Slovakia.Life (Basel, Switzerland) · 2023Article
- Bisphenols-A Threat to the Natural Environment.Materials (Basel, Switzerland) · 2023Review
- International Comparison, Risk Assessment, and Prioritisation of 26 Endocrine Disrupting Compounds in Three European River Catchments in the UK, Ireland, and Spain.Molecules (Basel, Switzerland) · 2023Article
- An Assessment of Mass Flows, Removal and Environmental Emissions of Bisphenols in a Sequencing Batch Reactor Wastewater Treatment Plant.Molecules (Basel, Switzerland) · 2022Article
- [Adsorption characteristics of six bisphenol compounds on magnetic three-dimensional nitrogen-doped carbon nanomaterials and their use in effervescent reaction-assisted dispersive microextraction].Se pu = Chinese journal of chromatography · 2022Article
- USAEME-GC/MS Method for Easy and Sensitive Determination of Nine Bisphenol Analogues in Water and Wastewater.Molecules (Basel, Switzerland) · 2022Article
- Diabetes mellitus: Plasticizers and nanomaterials acting as endocrine-disrupting chemicals (Review).Experimental and therapeutic medicine · 2022Review
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Authors and funding
2 authors at 1 institution in 1 country.
Funding
No grant is acknowledged in the PubMed record.
Abstract
The study focused on the application of GC in the quantitative analysis of bisphenols and their analogues (12 analytes), and the improvement of solid-phase extraction for the whole water analysis of complex water samples. The role of silylation in the qualitative and quantitative analysis of bisphenols was investigated. Partial degradation occurred for selected targets during hot injection with the presence of a silylation agent. A PSA (primary and secondary amines) sorbent placed on the top of the solid-phase extraction (SPE) column sorbent was found to be a matrix component trap, mostly for humic acids. The whole water analysis was performed by washing the filters with methanol and recycling the extract to the sample. The validation of SPE-GC/MS(SIM) gave limits of detection of 1-50 ng/L for ten target bisphenols with a method recovery of between 87 and 133%. The application of the method was tested by the analysis of wastewater sampled from three wastewater treatment plants located in Poland, and municipal surface waters. The only analytes found were BPA and BPS, within the range of 16-1465 ng/L and < MDL-1249 ng/L in wastewater, and 170-3113 ng/L and < MDL-1584 ng/L in surface water, respectively.
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