Evidence map›Paper›PMID 32381777›Full record

ArticleJournal of synchrotron radiation2020

Versatile compact heater design for in situ nano-tomography by transmission X-ray microscopy.

Stephen Antonelli, Arthur Ronne, Insung Han, Mingyuan Ge, Bobby Layne, Ashwin J Shahani, Kazuhiro Iwamatsu, James F Wishart, Steven L Hulbert, Wah Keat Lee and 2 more

Open access · bronzeAbstract read
In one paragraph

Article in Journal of synchrotron radiation, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
0.6field-weighted citation impact, top 41% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed, 14 citations in OpenAlex.

  1. Article
  2. Spatiotemporal mapping of alloy mesostructure dynamics via multimodal coherent X-ray diffraction imaging.Proceedings of the National Academy of Sciences of the United States of America · 2025
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

12 authors at 3 institutions in 1 country.

Stephen AntonelliNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.
Arthur RonneDepartment of Materials Science and Chemical Engineering, Stony Brook University, Stony Brook, NY 11794, USA.ORCID 0000-0001-7507-0757
Insung HanDepartment of Materials Science and Engineering, University of Michigan, Ann Arbor, MI 48109, USA.
Mingyuan GeNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.
Bobby LayneChemistry Division, Brookhaven National Laboratory, Upton, NY 11973, USA.
Ashwin J ShahaniDepartment of Materials Science and Engineering, University of Michigan, Ann Arbor, MI 48109, USA.
Kazuhiro IwamatsuChemistry Division, Brookhaven National Laboratory, Upton, NY 11973, USA.
James F WishartChemistry Division, Brookhaven National Laboratory, Upton, NY 11973, USA.ORCID 0000-0002-0488-7636
Steven L HulbertNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.ORCID 0000-0003-3127-6029
Wah Keat LeeNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.
Yu Chen Karen Chen-WiegartNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.ORCID 0000-0003-4445-2159
Xianghui XiaoNational Synchrotron Light Source II, Brookhaven National Laboratory, Upton, NY 11973, USA.ORCID 0000-0002-7142-3452
Brookhaven National Laboratory · USUniversity of Michigan · USStony Brook University · US

Funding

U.S. Department of Energy, Office of Science DE-SC0012704U.S. Department of Energy, Office of Science DE-SC0019118
6 · The paper itself

Abstract

A versatile, compact heater designed at National Synchrotron Light Source-II for in situ X-ray nano-imaging in a full-field transmission X-ray microscope is presented. Heater design for nano-imaging is challenging, combining tight spatial constraints with stringent design requirements for the temperature range and stability. Finite-element modeling and analytical calculations were used to determine the heater design parameters. Performance tests demonstrated reliable and stable performance, including maintaining the exterior casing close to room temperature while the heater is operating at above 1100°C, a homogenous heating zone and small temperature fluctuations. Two scientific experiments are presented to demonstrate the heater capabilities: (i) in situ 3D nano-tomography including a study of metal dealloying in a liquid molten salt extreme environment, and (ii) a study of pore formation in icosahedral quasicrystals. The progression of structural changes in both studies were clearly resolved in 3D, showing that the new heater enables powerful capabilities to directly visualize and quantify 3D morphological evolution of materials under real conditions by X-ray nano-imaging at elevated temperature during synthesis, fabrication and operation processes. This heater design concept can be applied to other applications where a precise, compact heater design is required.

Indexed as

in situ heatingmaterial characterizationsnano-tomographytransmission X-ray microscopes

Identifiers

PMID32381777
PMCPMC7285687
OpenAlexW3016877740

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.