Evidence map›Paper›PMID 32350618›Full record

ArticleMikrochimica acta2020

In situ growth of metal-organic framework HKUST-1 in an organic polymer as sorbent for nitrated and oxygenated polycyclic aromatic hydrocarbon in environmental water samples prior to quantitation by HPLC-UV.

Héctor Martínez-Pérez-Cejuela, María Guiñez, Ernesto F Simó-Alfonso, Pedro Amorós, Jamal El Haskouri, José M Herrero-Martínez

Open access · greenAbstract read
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In one paragraph

Article in Mikrochimica acta, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
1.6field-weighted citation impact, top 17% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed, 27 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors at 3 institutions in 2 countries.

Héctor Martínez-Pérez-CejuelaDepartment of Analytical Chemistry, University of Valencia, C/Dr. Moliner, 50, 46100, Burjassot, Valencia, Spain.ORCID https://orcid.org/0000-0002-6456-0846
María GuiñezInstituto de Química de San Luis (CCT-San Luis), Área de Química Analítica, Facultad de Química Bioquímica y Farmacia, Universidad Nacional de San Luis, Laboratorio de Espectrometría de Masas, Bloque III, Ejército de los Andes 950, CP5700, San Luis, Argentina.
Ernesto F Simó-AlfonsoDepartment of Analytical Chemistry, University of Valencia, C/Dr. Moliner, 50, 46100, Burjassot, Valencia, Spain.ORCID https://orcid.org/0000-0001-7502-6350
Pedro AmorósInstitute of Material Science (ICMUV), University of Valencia, Catedrático José Beltrán 2, 46980, Paterna, Valencia, Spain.ORCID https://orcid.org/0000-0002-8741-3769
Jamal El HaskouriInstitute of Material Science (ICMUV), University of Valencia, Catedrático José Beltrán 2, 46980, Paterna, Valencia, Spain.ORCID https://orcid.org/0000-0002-8895-1681
José M Herrero-MartínezDepartment of Analytical Chemistry, University of Valencia, C/Dr. Moliner, 50, 46100, Burjassot, Valencia, Spain. jmherrer@uv.es.ORCID https://orcid.org/0000-0002-8745-3795
Universitat de València · ESParc Científic de la Universitat de València · ESConsejo Nacional de Investigaciones Científicas y Técnicas · AR

Funding

Conselleria d'Educació, Investigació, Cultura i Esport PROMETEO/2016/145Ministerio de Ciencia, Innovación y Universidades RTI2018-095536-B-I00
6 · The paper itself

Abstract

An in situ preparation of metal-organic framework (HKUST-1) on the surface of an organic polymer is reported. The hybrid material was evaluated as sorbent for solid-phase extraction (SPE) of oxygenated and nitrated polycyclic aromatic hydrocarbons (PAHs). The growth of HKUST-1 on MAA-based polymer was accomplished using a layer-by-layer assembly strategy. The HKUST-1-polymer was characterized using powder X-ray diffraction and scanning electron microscopy to demonstrate the incorporation of MOF crystals onto the polymer surface. The MOF (nano)crystals were characterized using high-resolution transmission electron microscopy and high-angle annular-dark-field scanning transmission electron microscopy. The water-stable MOF-polymer was evaluated as SPE sorbent, and several variables that can influence the extraction recoveries of PAH derivatives were investigated. Under the selected conditions, the detection limits varied between 4 and 21 ng·L

Indexed as

Hybrid metal-organic framework-polymerNanoscale characterizationPAH derivativesPreconcentrationSolid-phase extractionSTEM-HAADFπ-Interaction

Identifiers

PMID32350618
OpenAlexW3021837314

What OpenQuestion holds

Textmetadata
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.