ArticleThe journal of physical chemistry. C, Nanomaterials and interfaces2020
Endogenous Dynamic Nuclear Polarization for Sensitivity Enhancement in Solid-State NMR of Electrode Materials.
Article in The journal of physical chemistry. C, Nanomaterials and interfaces, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 12 papers.
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Who cites it
12 citing papers in PubMed.
- Combined dynamic nuclear polarization and electron paramagnetic resonance at 0.34 T to investigate electrochemical lithium deposition on copper.Scientific reports · 2025Article
- Metal Ion Dynamic Nuclear Polarization in Mn(II)-Doped CdS Nanocrystals: Atomic-Scale Investigation of the Dopant and Its Host.ACS nano · 2025Article
- Composition and Structure of the solid electrolyte interphase on Na-Ion Anodes Revealed by Exo- and Endogenous Dynamic Nuclear Polarization─NMR Spectroscopy.Journal of the American Chemical Society · 2024Article
- Soliton Based Dynamic Nuclear Polarization: An Overhauser Effect in Cyclic Polyacetylene at High Field and Room Temperature.The journal of physical chemistry letters · 2024Article
- Endogenous metal-ion dynamic nuclear polarization for NMR signal enhancement in metal organic frameworks.Chemical science · 2023Article
- Polarizing agents for efficient high field DNP solid-state NMR spectroscopy under magic-angle spinning: from design principles to formulation strategies.Chemical science · 2023Review
- The Effect of Disorder on Endogenous MAS-DNP: Study of Silicate Glasses and Crystals.The journal of physical chemistry. C, Nanomaterials and interfaces · 2023Article
- Spin Hyperpolarization in Modern Magnetic Resonance.Chemical reviews · 2023Review
- Numerical recipes for faster MAS-DNP simulations.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2021Article
- Structure and Functionality of an Alkylated LiJournal of the American Chemical Society · 2021Article
- Site-specific dynamic nuclear polarization in a Gd(III)-labeled protein.Physical chemistry chemical physics : PCCP · 2020Article
- Enabling Natural AbundanceThe journal of physical chemistry letters · 2020Article
Corrections and comments
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Authors and funding
8 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Rational design of materials for energy storage systems relies on our ability to probe these materials at various length scales. Solid-state NMR spectroscopy is a powerful approach for gaining chemical and structural insights at the atomic/molecular level, but its low detection sensitivity often limits applicability. This limitation can be overcome by transferring the high polarization of electron spins to the sample of interest in a process called dynamic nuclear polarization (DNP). Here, we employ for the first time metal ion-based DNP to probe pristine and cycled composite battery electrodes. A new and efficient DNP agent, Fe(III), is introduced, yielding lithium signal enhancement up to 180 when substituted in the anode material Li
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.