Evidence map›Paper›PMID 32210164›Full record

ArticleToxins2020

Combined (d)SPE-QuEChERS Extraction of Mycotoxins in Mixed Feed Rations and Analysis by High Performance Liquid Chromatography-High-Resolution Mass Spectrometry.

Rocio Facorro, Maria Llompart, Thierry Dagnac

Open access · goldAbstract read
In one paragraph

Article in Toxins, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.

0numbers the graph read from it
0cells of the map it votes in
8citing papers in PubMed
3.9field-weighted citation impact, top 7% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

8 citing papers in PubMed, 27 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

3 authors at 2 institutions in 1 country.

Rocio FacorroGalician Agency for Food Quality-Agronomic and Agrarian Research Centre (AGACAL-CIAM), Unit of Organic Contaminants, Apartado 10, 15080 A Coruña, Spain.
Maria Llompart.Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, E-15782 Campus Vida, Universidad de Santiago de Compostela, 15782 Santiago de Compostela, Spain.
Thierry DagnacGalician Agency for Food Quality-Agronomic and Agrarian Research Centre (AGACAL-CIAM), Unit of Organic Contaminants, Apartado 10, 15080 A Coruña, Spain.
Universidade de Santiago de Compostela · ESCenter for Research in Agricultural Genomics · ES

Funding

Axencia Galega de Innovación Competitive Research Group GPC IN607B 2019/13Axencia Galega de Innovación Competitive Research Groups GPC 2017/04Axencia Galega de Innovación CONECTA-PEME GALAC project IN852A 2016/103CRETUS Strategic Partnership ED431E 2018/01Ministerio de Ciencia e Innovación IGDC13-1E-2026 (Infrastructure Program)
6 · The paper itself

Abstract

The objective of this work was the development of a methodology capable of simultaneously determine 26 mycotoxins in mixed feed rations collected in 20 dairy farms. A sample preparation methodology based on a combination of (d)SPE and QuEChERS extractions was used. Liquid chromatography-high resolution mass spectrometry was employed for both identification and quantification purposes. To this respect, a powerful workflow based on data-independent acquisition, consisting of fragmenting all precursor ions entering the mass spectrometer in narrow m/z isolation windows (SWATH), was implemented. SWATH data file then contains all the information that would be acquired in a multitude of different experimental approaches in a single all-encompassing dataset. Analytical method performance was evaluated in terms of linearity, repeatability and matrix effect. Relative recoveries were also measured, giving values above 80% for most compounds. Matrix-matched calibration was carried out and enabled reaching the low ng mL

Indexed as

Animal FeedAnimalsCattleChromatography, High Pressure LiquidDairyingFood ContaminationLimit of DetectionMass SpectrometryMycotoxinsReproducibility of ResultsSolid Phase ExtractionSpainMycotoxinsdata independent SWATHdispersive solid phase extractionhigh-resolution mass spectrometryliquid chromatographymixed feed rationsMycotoxinsQuEChERS

Identifiers

PMID32210164
PMCPMC7150789
OpenAlexW3014036568

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.