Evidence map›Paper›PMID 32045217›Full record

ArticleAnalytical chemistry2020

Surface Enhanced Raman Spectroscopy for Quantitative Analysis: Results of a Large-Scale European Multi-Instrument Interlaboratory Study.

Stefano Fornasaro, Fatima Alsamad, Monica Baia, Luís A E Batista de Carvalho, Claudia Beleites, Hugh J Byrne, Alessandro Chiadò, Mihaela Chis, Malama Chisanga, Amuthachelvi Daniel and 34 more

Abstract read
In one paragraph

Article in Analytical chemistry, 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 39 papers.

0numbers the graph read from it
0cells of the map it votes in
39citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

39 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

44 authors.

Stefano FornasaroRaman Spectroscopy Lab, Department of Engineering and Architecture, University of Trieste, P.le Europa 1, 34100 Trieste, Italy.ORCID 0000-0003-3057-7559
Fatima AlsamadUniversité de Reims Champagne-Ardenne, BioSpecT-EA7506, UFR de Pharmacie, 51 rue Cognacq-Jay, 51097 Reims, France.
Monica BaiaFaculty of Physics, Babes-Bolyai University, M. Kogalniceanu 1, 400084 Cluj-Napoca, Romania.
Luís A E Batista de CarvalhoMolecular-Physical Chemistry R&D Unit, Department of Chemistry, University of Coimbra, 3004-535 Coimbra, Portugal.ORCID 0000-0002-8059-8537
Claudia BeleitesChemometrix GmbH, Södeler Weg 19, 61200 Wölfersheim, Germany.
Hugh J ByrneFOCAS Research Institute, Technological University Dublin, Kevin Street, Dublin 8, Ireland.
Alessandro ChiadòDepartment of Applied Science and Technology, Politecnico di Torino, C.so Duca degli Abruzzi 24, 10129 Torino, Italy.ORCID 0000-0002-3230-8427
Mihaela ChisFaculty of Physics, Babes-Bolyai University, M. Kogalniceanu 1, 400084 Cluj-Napoca, Romania.
Malama ChisangaSchool of Chemistry, Manchester Institute of Biotechnology, University of Manchester, Manchester, United Kingdom M1 7DN.
Amuthachelvi DanielRadiation and Environmental Science Centre, FOCAS Research Institute, Technological University Dublin, Kevin Street, Dublin 8, Ireland.
Jakub DybasJagiellonian Centre for Experimental Therapeutics, Jagiellonian University, ul. Gronostajowa 2, 30-384 Krakow, Poland.
Gauthier EppeMass Spectrometry Laboratory (MSLab), MolSys RU, University of Liège, Liège, Belgium.
Guillaume FalgayracUniv. Lille, Univ. Littoral Côte d'Opale, EA 4490 - PMOI, F-59000 Lille, France.
Karen FauldsBionanotechnology Research Section, Department of Pure and Applied Chemistry, University of Strathclyde, 99 George Street, Glasgow, G1 1RD, United Kingdom.ORCID 0000-0002-5567-7399
Hrvoje GebaviCentre of Excellence for Advanced Materials and Sensing Devices, Division of Materials Physics, Rudjer Boskovic Institute, Bijenicka c. 54, 10000 Zagreb, Croatia.
Fabrizio GiorgisDepartment of Applied Science and Technology, Politecnico di Torino, C.so Duca degli Abruzzi 24, 10129 Torino, Italy.
Royston GoodacreDepartment of Biochemistry, Institute of Integrative Biology, University of Liverpool, Liverpool, United Kingdom, L69 7ZB.ORCID 0000-0003-2230-645X
Duncan GrahamBionanotechnology Research Section, Department of Pure and Applied Chemistry, University of Strathclyde, 99 George Street, Glasgow, G1 1RD, United Kingdom.
Pietro La MannaInstitute on Polymers, Composites and Biomaterials, National Research Council of Italy, via Campi Flegrei, 34, Pozzuoli, Naples 80078, Italy.
Stacey LaingBionanotechnology Research Section, Department of Pure and Applied Chemistry, University of Strathclyde, 99 George Street, Glasgow, G1 1RD, United Kingdom.
Lucio LittiNanostructures and Optics Laboratory, Department of Chemical Sciences, University of Padova, Via Marzolo 1 - 35131, Padova, Italy.ORCID 0000-0001-6247-5456
Fiona M LyngRadiation and Environmental Science Centre, FOCAS Research Institute, Technological University Dublin, Kevin Street, Dublin 8, Ireland.
Kamilla MalekJagiellonian Centre for Experimental Therapeutics, Jagiellonian University, ul. Gronostajowa 2, 30-384 Krakow, Poland.ORCID 0000-0003-0582-2743
Cedric MalherbeMass Spectrometry Laboratory (MSLab), MolSys RU, University of Liège, Liège, Belgium.
Maria P M MarquesMolecular-Physical Chemistry R&D Unit, Department of Chemistry, University of Coimbra, 3004-535 Coimbra, Portugal.ORCID 0000-0002-8391-0055
Moreno MeneghettiNanostructures and Optics Laboratory, Department of Chemical Sciences, University of Padova, Via Marzolo 1 - 35131, Padova, Italy.ORCID 0000-0003-3355-4811
Elisa MitriRaman Spectroscopy Lab, Department of Engineering and Architecture, University of Trieste, P.le Europa 1, 34100 Trieste, Italy.
Vlasta Mohaček-GroševCentre of Excellence for Advanced Materials and Sensing Devices, Division of Materials Physics, Rudjer Boskovic Institute, Bijenicka c. 54, 10000 Zagreb, Croatia.
Carlo MorassoNanomedicine and Molecular Imaging Lab, Istituti Clinici Scientifici Maugeri IRCCS, Via Maugeri 4, 27100 Pavia, Italy.
Howbeer MuhamadaliDepartment of Biochemistry, Institute of Integrative Biology, University of Liverpool, Liverpool, United Kingdom, L69 7ZB.
Pellegrino MustoInstitute on Polymers, Composites and Biomaterials, National Research Council of Italy, via Campi Flegrei, 34, Pozzuoli, Naples 80078, Italy.
Chiara NovaraDepartment of Applied Science and Technology, Politecnico di Torino, C.so Duca degli Abruzzi 24, 10129 Torino, Italy.
Marianna PannicoInstitute on Polymers, Composites and Biomaterials, National Research Council of Italy, via Campi Flegrei, 34, Pozzuoli, Naples 80078, Italy.
Guillaume PenelUniv. Lille, Univ. Littoral Côte d'Opale, EA 4490 - PMOI, F-59000 Lille, France.
Olivier PiotUniversité de Reims Champagne-Ardenne, BioSpecT-EA7506, UFR de Pharmacie, 51 rue Cognacq-Jay, 51097 Reims, France.
Tomas RindzeviciusTechnical University of Denmark, Department of Health Technology, Ørsteds Plads, Building 345C, DK-2800 Kgs. Lyngby, Denmark.
Elena A RusuFaculty of Physics, Babes-Bolyai University, M. Kogalniceanu 1, 400084 Cluj-Napoca, Romania.
Michael S SchmidtSilmeco ApS, Kenny Drews Vej 101, 2450 Copenhagen, Denmark.
Valter SergoRaman Spectroscopy Lab, Department of Engineering and Architecture, University of Trieste, P.le Europa 1, 34100 Trieste, Italy.
Ganesh D SockalingumUniversité de Reims Champagne-Ardenne, BioSpecT-EA7506, UFR de Pharmacie, 51 rue Cognacq-Jay, 51097 Reims, France.
Valérie UntereinerUniversité de Reims Champagne-Ardenne, BioSpecT-EA7506, UFR de Pharmacie, 51 rue Cognacq-Jay, 51097 Reims, France.
Renzo VannaNanomedicine and Molecular Imaging Lab, Istituti Clinici Scientifici Maugeri IRCCS, Via Maugeri 4, 27100 Pavia, Italy.ORCID 0000-0001-6218-8393
Ewelina WiercigrochJagiellonian Centre for Experimental Therapeutics, Jagiellonian University, ul. Gronostajowa 2, 30-384 Krakow, Poland.
Alois BonifacioRaman Spectroscopy Lab, Department of Engineering and Architecture, University of Trieste, P.le Europa 1, 34100 Trieste, Italy.ORCID 0000-0002-2251-7786

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Surface-enhanced Raman scattering (SERS) is a powerful and sensitive technique for the detection of fingerprint signals of molecules and for the investigation of a series of surface chemical reactions. Many studies introduced quantitative applications of SERS in various fields, and several SERS methods have been implemented for each specific application, ranging in performance characteristics, analytes used, instruments, and analytical matrices. In general, very few methods have been validated according to international guidelines. As a consequence, the application of SERS in highly regulated environments is still considered risky, and the perception of a poorly reproducible and insufficiently robust analytical technique has persistently retarded its routine implementation. Collaborative trials are a type of interlaboratory study (ILS) frequently performed to ascertain the quality of a single analytical method. The idea of an ILS of quantification with SERS arose within the framework of Working Group 1 (WG1) of the EU COST Action BM1401 Raman4Clinics in an effort to overcome the problematic perception of quantitative SERS methods. Here, we report the first interlaboratory SERS study ever conducted, involving 15 laboratories and 44 researchers. In this study, we tried to define a methodology to assess the reproducibility and trueness of a quantitative SERS method and to compare different methods. In our opinion, this is a first important step toward a "standardization" process of SERS protocols, not proposed by a single laboratory but by a larger community.

Identifiers

PMID32045217
PMCPMC7997108

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.