ArticleNanomaterials (Basel, Switzerland)2020
Tailorable Synthesis of Highly Oxidized Graphene Oxides via an Environmentally-Friendly Electrochemical Process.
Article in Nanomaterials (Basel, Switzerland), 2020. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 13 papers.
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Who cites it
13 citing papers in PubMed.
- Electrochemical intercalation of anions into graphite: Fundamental aspects, material synthesis, and application to the cathode of dual-ion batteries.ChemistryOpen · 2024Review
- Reduced graphene oxide/zinc oxide composite as an electrochemical sensor for acetylcholine detection.Scientific reports · 2024Article
- The Influence of Reaction Conditions on the Properties of Graphene Oxide.Nanomaterials (Basel, Switzerland) · 2024Article
- Article
- Machine Learning for Property Prediction and Optimization of Polymeric Nanocomposites: A State-of-the-Art.International journal of molecular sciences · 2022Review
- PMMA-Based Nanocomposites for Odontology Applications: A State-of-the-Art.International journal of molecular sciences · 2022Review
- Review
- Graphene-Based Polymer Composites for Flexible Electronic Applications.Micromachines · 2022Review
- Editorial for "Properties and Applications of Graphene and Its Derivatives".Nanomaterials (Basel, Switzerland) · 2022Article
- Graphene Oxide Chemistry Management via the Use of KMnONanomaterials (Basel, Switzerland) · 2021Article
- Graphene-Based Sensors for the Detection of Bioactive Compounds: A Review.International journal of molecular sciences · 2021Review
- Graphene Oxides Derivatives Prepared by an Electrochemical Approach: Correlation between Structure and Properties.Nanomaterials (Basel, Switzerland) · 2020Article
- Antibacterial Action of Nanoparticle Loaded Nanocomposites Based on Graphene and Its Derivatives: A Mini-Review.International journal of molecular sciences · 2020Review
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Authors and funding
5 authors.
Funding
Abstract
Graphene oxide (GO) is an attractive alternative to graphene for many applications due to its captivating optical, chemical, and electrical characteristics. In this work, GO powders with a different amount of surface groups were synthesized from graphite via an electrochemical two-stage process. Many synthesis conditions were tried to maximize the oxidation level, and comprehensive characterization of the resulting samples was carried out via elemental analysis, microscopies (TEM, SEM, AFM), X-ray diffraction, FT-IR and Raman spectroscopies as well as electrical resistance measurements. SEM and TEM images corroborate that the electrochemical process used herein preserves the integrity of the graphene flakes, enabling to obtain large, uniform and well exfoliated GO sheets. The GOs display a wide range of C/O ratios, determined by the voltage and time of each stage as well as the electrolyte concentration, and an unprecedented minimum C/O value was obtained for the optimal conditions. FT-IR evidences strong intermolecular interactions between neighbouring oxygenated groups. The intensity ratio of D/G bands in the Raman spectra is high for samples prepared using concentrated H
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