Evidence map›Paper›PMID 31796786›Full record

ArticleScientific reports2019

Single-pass STEM-EMCD on a zone axis using a patterned aperture: progress in experimental and data treatment methods.

Thomas Thersleff, Linus Schönström, Cheuk-Wai Tai, Roman Adam, Daniel E Bürgler, Claus M Schneider, Shunsuke Muto, Ján Rusz

Abstract read
In one paragraph

Article in Scientific reports, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Thomas ThersleffStockholm University, Department of Materials and Environmental Chemistry, 10691, Stockholm, Sweden. thomas.thersleff@mmk.su.se.
Linus SchönströmStockholm University, Department of Materials and Environmental Chemistry, 10691, Stockholm, Sweden.
Cheuk-Wai TaiStockholm University, Department of Materials and Environmental Chemistry, 10691, Stockholm, Sweden.
Roman AdamForschungszentrum Jülich GmbH, Peter Grünberg Institut, D-52425, Jülich, Germany.
Daniel E BürglerForschungszentrum Jülich GmbH, Peter Grünberg Institut, D-52425, Jülich, Germany.
Claus M SchneiderForschungszentrum Jülich GmbH, Peter Grünberg Institut, D-52425, Jülich, Germany.
Shunsuke MutoNagoya University, Institute of Materials and Systems for Sustainability, Nagoya, 464-8603, Japan.
Ján RuszUppsala University, Department of Physics and Astronomy, Box 516, 75120, Uppsala, Sweden.

Funding

Stiftelsen för Strategisk Forskning, Sweden ITM17-0301Vetenskapsrådet 2016-05113Vetenskapsrådet 2017-04026
6 · The paper itself

Abstract

Measuring magnetic moments in ferromagnetic materials at atomic resolution is theoretically possible using the electron magnetic circular dichroism (EMCD) technique in a (scanning) transmission electron microscope ((S)TEM). However, experimental and data processing hurdles currently hamper the realization of this goal. Experimentally, the sample must be tilted to a zone-axis orientation, yielding a complex distribution of magnetic scattering intensity, and the same sample region must be scanned multiple times with sub-atomic spatial registration necessary at each pass. Furthermore, the weak nature of the EMCD signal requires advanced data processing techniques to reliably detect and quantify the result. In this manuscript, we detail our experimental and data processing progress towards achieving single-pass zone-axis EMCD using a patterned aperture. First, we provide a comprehensive data acquisition and analysis strategy for this and other EMCD experiments that should scale down to atomic resolution experiments. Second, we demonstrate that, at low spatial resolution, promising EMCD candidate signals can be extracted, and that these are sensitive to both crystallographic orientation and momentum transfer.

Identifiers

PMID31796786
PMCPMC6890689

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.