Evidence map›Paper›PMID 31744228›Full record

ArticleMaterials (Basel, Switzerland)2019

Synthesis of Colloidal Au Nanoparticles through Ultrasonic Spray Pyrolysis and Their Use in the Preparation of Polyacrylate-AuNPs' Composites.

Doris Golub, Andrej Ivanič, Peter Majerič, Hanuma Reddy Tiyyagura, Ivan Anžel, Rebeka Rudolf

Abstract read
In one paragraph

Article in Materials (Basel, Switzerland), 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.

0numbers the graph read from it
0cells of the map it votes in
7citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

7 citing papers in PubMed.

  1. Review
  2. Article
  3. Study of Ni/YMaterials (Basel, Switzerland) · 2023
    Article
  4. Article
  5. Review
  6. Article
  7. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Doris GolubZlatarna Celje d. o. o., Kersnikova 19, 3000 Celje, Slovenia.
Andrej IvaničFaculty of Civil Engineering, Transportation Engineering and Architecture, University of Maribor, Smetanova ulica 17, 2000 Maribor, Slovenia.ORCID 0000-0002-6974-1224
Peter MajeričFaculty of Mechanical Engineering, University of Maribor, Smetanova ulica 17, 2000 Maribor, Slovenia.
Hanuma Reddy TiyyaguraZlatarna Celje d. o. o., Kersnikova 19, 3000 Celje, Slovenia.
Ivan AnželFaculty of Mechanical Engineering, University of Maribor, Smetanova ulica 17, 2000 Maribor, Slovenia.
Rebeka RudolfZlatarna Celje d. o. o., Kersnikova 19, 3000 Celje, Slovenia.ORCID 0000-0003-0510-5752

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Colloidal gold nanoparticles (AuNPs) were prepared from two different liquid precursors (gold (III) acetate and gold (III) chloride), using the Ultrasonic Spray Pyrolysis (USP) process. The STEM characterisation showed that the AuNPs from gold chloride are spherical, with average diameters of 57.2 and 69.4 nm, while the AuNPs from gold acetate are ellipsoidal, with average diameters of 84.2 and 134.3 nm, according to Dynamic Light Scattering (DLS) measurements. UV/VIS spectroscopy revealed the maximum absorbance band of AuNPs between 532 and 560 nm, which indicates a stable state. Colloidal AuNPs were used as starting material and were mixed together with acrylic acid (AA) and acrylamide (Am) for the free radical polymerization of polyacrylate-AuNPs' composites, with the purpose of using them for temporary cavity fillings in the dental industry. SEM characterisation of polyacrylate-AuNPs' composites revealed a uniform distribution of AuNPs through the polymer matrix, revealing that the AuNPs remained stable during the polymerization process. The density measurements revealed that colloidal AuNPs increase the densities of the prepared polyacrylate-AuNPs' composites; the densities were increased up to 40% in comparison with the densities of the control samples. A compressive test showed that polyacrylate-AuNPs' composites exhibited lower compressive strength compared to the control samples, while their toughness increased. At 50% compression deformation some of the samples fracture, suggesting that incorporation of colloidal AuNPs do not improve their compressive strength, but increase their toughness significantly. This increased toughness is the measured property which makes prepared polyacrylate-AuNPs potentially useful in dentistry.

Indexed as

characterizationcolloidal gold nanoparticlespolyacrylate compositesUltrasonic Spray Pyrolysis

Identifiers

PMID31744228
PMCPMC6888614

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.