ArticleMaterials (Basel, Switzerland)2019
Preparation of Reswellable Amorphous Porous Celluloses through Hydrogelation from Ionic Liquid Solutions.
Article in Materials (Basel, Switzerland), 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.
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Who cites it
2 citing papers in PubMed, 13 citations in OpenAlex.
- Recent Advances in Cellulose-Based Hydrogels Prepared by Ionic Liquid-Based Processes.Gels (Basel, Switzerland) · 2023Review
- Insights on Some Polysaccharide Gel Type Materials and Their Structural Peculiarities.Gels (Basel, Switzerland) · 2022Review
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Authors and funding
5 authors at 1 institution in 1 country.
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Abstract
In this study, we have performed the preparation of reswellable amorphous porous celluloses through regeneration from hydrogels. The cellulose hydrogels were first prepared from solutions with an ionic liquid, 1-butyl-3-methylimidazolium chloride (BMIMCl), in different concentrations. Lyophilization of the hydrogels efficiently produced the regenerated celluloses. The powder X-ray diffraction and scanning electron microscopic measurements of the products suggest an amorphous structure and porous morphology, respectively. Furthermore, the pore sizes of the regenerated celluloses, or in turn, the network sizes of cellulose chains in the hydrogels, were dependent on the concentrations of the initially prepared solutions with BMIMCl, which also affected the tensile mechanical properties. It was suggested that the dissolution states of the cellulose chains in the solutions were different, in accordance with the concentrations, which representatively dominated the pore and network sizes of the above materials. When the porous celluloses were immersed in water, reswelling was observed to regenerate the hydrogels.
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