Evidence map›Paper›PMID 31505305›Full record

ArticleJournal of magnetic resonance (San Diego, Calif. : 1997)2019

Modular, triple-resonance, transmission line DNP MAS probe for 500 MHz/330 GHz.

Marcel Reese, Christy George, Chen Yang, Sudheer Jawla, J Tassilo Grün, Harald Schwalbe, Christina Redfield, Richard J Temkin, Robert G Griffin

Abstract read
In one paragraph

Article in Journal of magnetic resonance (San Diego, Calif. : 1997), 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed.

  1. A complete 3D-printed tool kit for Solid-State NMR sample and rotor handling.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2024
    Article
  2. 3D-printed stators & drive caps for magic-angle spinning NMR.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2022
    Article
  3. Article
  4. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Marcel ReeseDepartment of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, United States.
Christy GeorgeDepartment of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, United States.
Chen YangDepartment of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, United States.
Sudheer JawlaPlasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, MA 02139, United States.
J Tassilo GrünInstitute for Organic Chemistry and Chemical Biology, Center for Biomolecular Magnetic Resonance, Johann Wolfgang Goethe-Universität Frankfurt, 60438 Frankfurt, Germany.
Harald SchwalbeInstitute for Organic Chemistry and Chemical Biology, Center for Biomolecular Magnetic Resonance, Johann Wolfgang Goethe-Universität Frankfurt, 60438 Frankfurt, Germany.
Christina RedfieldDepartment of Biochemistry, University of Oxford, South Parks Road, Oxford OX1 3QU, United Kingdom.
Richard J TemkinPlasma Science and Fusion Center, Massachusetts Institute of Technology, Cambridge, MA 02139, United States; Department of Physics, Massachusetts Institute of Technology, Cambridge, MA 02139, United States.
Robert G GriffinDepartment of Chemistry and Francis Bitter Magnet Laboratory, Massachusetts Institute of Technology, Cambridge, MA 02139, United States. Electronic address: rgg@mit.edu.

Funding

OverallP41EB002026 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2003 to 2018
$17.9M
High Field DNP in Biological SystemsR01EB002804 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2003 to 2018
$9.1M
Tunable 330 GHz Gyrotron for DNP/NMRR01EB004866 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI TEMKIN, RICHARD J · 2006 to 2024
$7.9M
High Power Millimeter Wave/Terahertz Sources for Magnetic ResonanceR01EB001965 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI TEMKIN, RICHARD J · 2003 to 2021
$7.8M
Acquisition of a 900 MHz NMR SpectrometerP41GM066360 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2002 to 2006
$6.7M
Solid State NMR Studies of Peptides and ProteinsR01EB003151 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2004 to 2015
$6.5M
Solid State NMR Studies of Membrane ProteinsR01EB001960 · NIBIB · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2003 to 2017
$6.5M
High Field DNP and EPR in Biological SystemsR01GM132997 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2019 to 2025
$4.6M
TR&D 4 -- Advanced Magic Angle Spinning NMR methodsP41GM132079 · NIGMS · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2019 to 2021
$3.6M
800 MHz Low Temperature Magic Angle Spinning NMR Probe.S10RR027895 · NCRR · MASSACHUSETTS INSTITUTE OF TECHNOLOGY · PI GRIFFIN, ROBERT GUY · 2009 to 2009
$300k
NCRR NIH HHS S10 RR027895NIBIB NIH HHS P41 EB002026NIBIB NIH HHS R01 EB001960NIBIB NIH HHS R01 EB001965NIBIB NIH HHS R01 EB002804NIBIB NIH HHS R01 EB003151NIBIB NIH HHS R01 EB004866NIGMS NIH HHS P41 GM066360NIGMS NIH HHS P41 GM132079NIGMS NIH HHS R01 GM132997
6 · The paper itself

Abstract

We describe the design and construction of a modular, triple-resonance, fully balanced, DNP-MAS probe based on transmission line technology and its integration into a 500 MHz/330 GHz DNP-NMR spectrometer. A novel quantitative probe design and characterization strategy is developed and employed to achieve optimal sensitivity, RF homogeneity and excellent isolation between channels. The resulting three channel HCN probe has a modular design with each individual, swappable module being equipped with connectorized, transmission line ports. This strategy permits attachment of a mating connector that facilitates accurate impedance measurements at these ports and allows characterization and adjustment (e.g. for balancing or tuning/matching) of each component individually. The RF performance of the probe is excellent; for example, the

Indexed as

CyclotronsElectric ImpedanceEquipment DesignIndicators and ReagentsMicrowavesMuramidaseNuclear Magnetic Resonance, BiomolecularRNAUreaIndicators and ReagentsMuramidaseRNAUreaBalanced transmission line probeNMR probe characterizationNovel probe designSolid state DNP

Identifiers

PMID31505305
PMCPMC6766420

What OpenQuestion holds

Textmetadata
LicenceTDM
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.