ArticleBeilstein journal of organic chemistry2019
Reaction of oxiranes with cyclodextrins under high-energy ball-milling conditions.
Article in Beilstein journal of organic chemistry, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.
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Who cites it
7 citing papers in PubMed.
- Mechanochemical Degradation of Biopolymers.Molecules (Basel, Switzerland) · 2023Review
- Comparison of the Conventional and Mechanochemical Syntheses of Cyclodextrin Derivatives.Molecules (Basel, Switzerland) · 2023Review
- Investigation of the Drug Carrier Properties of Insoluble Cyclodextrin Polymer Microspheres.Biomolecules · 2022Article
- Toward a Greener World-Cyclodextrin Derivatization by Mechanochemistry.Molecules (Basel, Switzerland) · 2021Review
- Research Progress on Synthesis and Application of Cyclodextrin Polymers.Molecules (Basel, Switzerland) · 2021Review
- New Lipidyl-Cyclodextrins Obtained by Ring Opening of Methyl Oleate Epoxide Using Ball Milling.Biomolecules · 2020Article
- Particle size effect in the mechanically assisted synthesis of β-cyclodextrin mesitylene sulfonate.Beilstein journal of organic chemistry · 2020Article
Corrections and comments
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Authors and funding
6 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
This work presents a proof of concept for a green cyclodextrin derivatisation method that uses low-boiling epoxide reagents in a high-energy ball mill (HEBM). The simplified preparation and purification of low substitution-degree common (2-hydroxy)propylated β- and γ-cyclodextrins (β/γ-CDs) has been realised. The intelligent use of propylene oxide has also facilitated the more effective synthesis of highly substituted γ-CD. Epichlorohydrin-crosslinked CD-polymers (CDPs) have also been effectively prepared in the ball mill. The unoptimised preparations of soluble and insoluble CDPs displayed very small particle size distributions, while the prepared polymers currently have different complexation properties to those of their classically prepared analogues.
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Registered trials
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