Evidence map›Paper›PMID 31293669›Full record

ArticleBeilstein journal of organic chemistry2019

Mechanochemical amorphization of chitin: impact of apparatus material on performance and contamination.

Thomas Di Nardo, Audrey Moores

Abstract read
In one paragraph

Article in Beilstein journal of organic chemistry, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.

0numbers the graph read from it
0cells of the map it votes in
5citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

5 citing papers in PubMed.

  1. Article
  2. Article
  3. Article
  4. The mechanochemical synthesis of polymers.Chemical Society reviews · 2022
    Review
  5. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

2 authors.

Thomas Di NardoCentre in Green Chemistry and Catalysis, Department of Chemistry, McGill University, 801 Sherbrooke St. West, Montreal, QC, H3A 0B8, Canada.ORCID 0000-0003-3696-8470
Audrey MooresCentre in Green Chemistry and Catalysis, Department of Chemistry, McGill University, 801 Sherbrooke St. West, Montreal, QC, H3A 0B8, Canada.ORCID 0000-0003-1259-913X

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Herein, we present a study of the impact of the jar and ball medium on the performance in the mechanochemical amorphization of chitin. We measured the crystallinity index of chitin after milling it in a vibration mill in an apparatus made of copper, aluminum, brass, tungsten carbide, zirconia, stainless steel, polytetrafluoroethylene (PTFE), or poly(methyl methacrylate) (PMMA). These materials offer a range of Vickers hardness values and the impact of these parameters is discussed. The role of the size and mass of the balls is also studied in the case of stainless steel. This study also highlights one of the major challenges during milling, which is contamination of the studied samples.

Indexed as

amorphizationbiomasschitinhardnessmechanochemistrymetal contamination

Identifiers

PMID31293669
PMCPMC6604705

What OpenQuestion holds

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LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.