Evidence map›Paper›PMID 30974571›Full record

ArticlePolymers2016

Optimized Synthesis According to One-Step Process of a Biobased Thermoplastic Polyacetal Derived from Isosorbide.

Nadia Hammami, Nathalie Jarroux, Mike Robitzer, Mustapha Majdoub, Jean-Pierre Habas

Open access · goldAbstract read
In one paragraph

Article in Polymers, 2016. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
0.7field-weighted citation impact, top 27% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 18 citations in OpenAlex.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors at 3 institutions in 2 countries.

Nadia HammamiInstitut Charles Gerhardt, CC 1702, Place E. Bataillon, 34095 Montpellier, France. nadia.hammami@etu.umontpellier.fr.
Nathalie JarrouxLaboratoire Analyse et Modélisation pour la Biologie et l'Environnement, UMR 8587, Université d'Evry-Val d'Essonne, 91025 Evry, France. nathalie.jarroux@univ-evry.fr.
Mike RobitzerInstitut Charles Gerhardt, CC 1702, Place E. Bataillon, 34095 Montpellier, France. mike.robitzer@enscm.fr.
Mustapha MajdoubLaboratoire des Interfaces et Matériaux Avancés, Université de Monastir, 5000 Monastir, Tunisia. mustapha.majdoub@fsm.rnu.tn.
Jean-Pierre HabasInstitut Charles Gerhardt, CC 1702, Place E. Bataillon, 34095 Montpellier, France. jean-pierre.habas@umontpellier.fr.
Institut Charles Gerhardt Montpellier · FRUniversity of Monastir · TNUniversité d'Évry Val-d'Essonne · FR

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This paper describes both the synthesis and characterization of a biobased and non-aromatic polyacetal produced from the reaction between isosorbide and methylene chloride. The reaction was conducted in an aprotic dipolar and harmless solvent using a one-step, fast and economical procedure. The chemical composition of this polymer was investigated using Nuclear Magnetic Resonance and Fourier Transform Infra-Red spectroscopies. The molecular weights were examined by size exclusion chromatography and MALDI-TOF spectrometry. The synthesis conditions (concentration, mixing speed, solvent nature, stoichiometry, addition mode of one reactan) were found to strongly influence both polymer architecture and reaction yield. Under moderated stirring conditions, the polyacetal was characterized by a larger amount of macro-cycles. Inversely, under higher intensity mixing and with an excess of methylene chloride, it was mainly composed of linear chains. In this latter case, the polymeric material presented an amorphous morphology with a glass transition temperature (

Indexed as

biosourced polymercyclic/linear architecturesisosorbidephysicochemical propertiespolyacetalspectroscopiessynthesis optimization

Identifiers

PMID30974571
PMCPMC6431881
OpenAlexW2478013714

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.