ArticlePolymers2019
Facile Synthesis of Methylsilsesquioxane Aerogels with Uniform Mesopores by Microwave Drying.
Article in Polymers, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.
What it found
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Who cites it
6 citing papers in PubMed.
- Robust and Thermally Stable Silicone Aerogels with Hyperconnected Network via Kinetically Optimized Hyperbranched Silane Precursors.Advanced science (Weinheim, Baden-Wurttemberg, Germany) · 2026Article
- InGaN Laser Diode with Spin-on-Glass Isolation Fabricated by Planarization and Etch-Back Process.Micromachines · 2026Article
- Development of a Bio-Inspired Aerogel with Robust Sustainability and Thermal Insulation Performance.Materials (Basel, Switzerland) · 2025Article
- Cost-Effective Preparation of Hydrophobic and Thermal-Insulating Silica Aerogels.Nanomaterials (Basel, Switzerland) · 2024Article
- Rapid Preparation of Mesoporous Methylsilsesquioxane Aerogels by Microwave Heating Technology.Molecules (Basel, Switzerland) · 2021Article
- Mechanically strong polyimide aerogels cross-linked with low-cost polymers.RSC advances · 2021Article
Corrections and comments
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Authors and funding
6 authors.
Funding
Abstract
Methylsilsesquioxane (MSQ) aerogels with uniform mesopores were facilely prepared via a sol⁻gel process followed by microwave drying with methyltrimethoxysilane (MTMS) as a precursor, hydrochloric acid (HCl) as a catalyst, water and methanol as solvents, hexadecyltrimethylammonium chloride (CTAC) as a surfactant and template, and propylene oxide (PO) as a gelation agent. The microstructure, chemical composition, and pore structures of the resultant MSQ aerogels were investigated in detail to achieve controllable preparation of MSQ aerogels, and the thermal stability of MSQ aerogels was also analyzed. The gelation agent, catalyst, solvent, and microwave power have important roles related to the pore structures of MSQ aerogels. Meanwhile, the microwave drying method was found to not only have a remarkable effect on improving production efficiency, but also to be conducive to avoiding the collapse of pore structure (especially micropores) during drying. The resulting MSQ aerogel microwave-dried at 500 W possessed a specific surface area up to 821 m²/g and a mesopore size of 20 nm, and displayed good thermal stability.
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Registered trials
Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.