ArticlePolymers2019
Non-Isothermal Crystallization Behavior of PEEK/Graphene Nanoplatelets Composites from Melt and Glass States.
Article in Polymers, 2019. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 14 papers.
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Who cites it
14 citing papers in PubMed.
- Article
- Drug Delivery Device Design and Compatibility with Nitrogen Dioxide Gas Sterilization.Pharmaceuticals (Basel, Switzerland) · 2025Article
- Article
- Unraveling the Print-Structure-Property Relationships in the FFF of PEEK: A Critical Assessment of Print Parameters.Polymers · 2025Article
- Article
- Revolutionizing Dental Polymers: The Versatility and Future Potential of Polyetheretherketone in Restorative Dentistry.Polymers · 2024Review
- Engineering the Crystalline Architecture for Enhanced Properties in Fast-Rate Processing of Poly(ether ether ketone) (PEEK) Nanocomposites.ACS applied engineering materials · 2024Article
- Article
- Determination of Shear Bond Strength between PEEK Composites and Veneering Composites for the Production of Dental Restorations.Materials (Basel, Switzerland) · 2023Article
- Article
- Understanding the Reinforcement of Graphene in Poly(Ether Ether Ketone)/Carbon Fibre Laminates.Polymers · 2021Article
- Comprehensive Enhancement in Thermomechanical Performance of Melt-Extruded PEEK Filaments by Graphene Incorporation.Polymers · 2021Article
- Production of graphene nanoplate/polyetheretherketone composites by semi-industrial melt-compounding.Heliyon · 2020Article
- A Novel Class of Cost Effective and High Performance Composites Based on Terephthalate Salts Reinforced Polyether Ether Ketone.Polymers · 2019Article
Corrections and comments
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Authors and funding
5 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
The effect of the graphene nanoplateletets (GNP), at concentration of 1, 5 and 10 wt %, in Poly ether ether ketone (PEEK) composite crystallization from melt and during cold crystallization were investigated by differential scanning calorimetry (DSC) and real time X-ray diffraction experiments. DSC results revealed a double effect of GNP: (a) nucleating effect crystallization from melt started at higher temperatures and (b) longer global crystallization time due to the restriction in the polymer chain mobility. This hindered mobility were proved by rheological behavior of nanocomposites, because to the increase of complex viscosity, G', G″ with the GNP content, as well as the non-Newtonian behavior found in composites with high GNP content. Finally, real time wide and small angle synchrotron X-ray radiation (WAXS/SAXS) X-ray measurements showed that GNP has not affected the orthorhombic phase of PEEK nor the evolution of the crystal phase during the crystallization processes. However, the correlation length of the crystal obtained by WAXS and the long period (L) by SAXS varied depending on the GNP content.
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